User:Megan L. Channell/Notebook/Masters Research/2013/11/21: Difference between revisions
From OpenWetWare
No edit summary |
|||
| Line 9: | Line 9: | ||
* The last time I did DSC, it could not finish because there was not enough nitrogen. I made new samples and re-run them. The new samples I made were the 0, 0.1, 0.5, 1, 5, and 10% but this time, I added the MOF-5 and the solvent together and sonicated them. Once they were fully dissolved, I put the PLA in and sonicated them. Once everything was fully dissolved I poured them into the molds and let them sit overnight. | * The last time I did DSC, it could not finish because there was not enough nitrogen. I made new samples and re-run them. The new samples I made were the 0, 0.1, 0.5, 1, 5, and 10% but this time, I added the MOF-5 and the solvent together and sonicated them. Once they were fully dissolved, I put the PLA in and sonicated them. Once everything was fully dissolved I poured them into the molds and let them sit overnight. | ||
#0.1 %, 0.5 %, 1.0 %, 5.0 %, 10 % and 0 % w/v. | |||
##0.1 % - 1.0001 g PLA, 0.001 g MOF-5, 10 mL dichloromethane | |||
##0.5 % - 0.9944 g PLA, 0.0048 g MOF-5, 10 mL dichloromethane | |||
##1.0 % - 0.9903 g PLA, 0.0097 g MOF-5, 10 mL dichloromethane | |||
##5.0 % - 0.509 g PLA, 0.0495 g MOF-5, 10 mL dichloromethane | |||
##10.0 % - 0.8993 g PLA, 0.999 g MOF-5, 10 mL dichloromethane | |||
##0 % - 0.9998 g PLA, 10 mL dichloromethane | |||
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### --> | <!-- ##### DO NOT edit below this line unless you know what you are doing. ##### --> | ||
|} | |} | ||
__NOTOC__ | __NOTOC__ | ||
Revision as of 14:03, 22 November 2013
 Project name
|
<html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
DSC and new samples
| |
