User:Megan L. Channell/Notebook/Masters Research/2014/02/27

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Current revision (21:05, 30 March 2014) (view source)
(AuNp Citrate)
 
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Data from [[User:Megan L. Channell/Notebook/Masters Research/2014/02/10| February 2]]
Data from [[User:Megan L. Channell/Notebook/Masters Research/2014/02/10| February 2]]
*[[Image:MOF-5 ABS 2 10 2014 DSC.png]]
*[[Image:MOF-5 ABS 2 10 2014 DSC.png]]
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*[[Image:MOF 5 ABS 3 4 14.png]]
==AuNp Citrate==
==AuNp Citrate==
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* let it boil than added 3 mL of sodium citrate and continue to boil for 40 mins
* let it boil than added 3 mL of sodium citrate and continue to boil for 40 mins
**citrate= 0.1010 g in 10 mL
**citrate= 0.1010 g in 10 mL
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==Note==
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Did not get that many mL's so I will redo it on the February 28. I had it in the hood, and instead it should have been on the bench with a watch glass over it.

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Data

Data from February 2

  • Image:MOF-5 ABS 2 10 2014 DSC.png
  • Image:MOF 5 ABS 3 4 14.png

AuNp Citrate

  • Protocol taken from Dr. Hartings
  • Doubled the initial volume to 100 mL
  • .011g in 25mL than placed 22.31 mL of this into a 100 mL volumetric flask and diluted
  • let it boil than added 3 mL of sodium citrate and continue to boil for 40 mins
    • citrate= 0.1010 g in 10 mL

Note

Did not get that many mL's so I will redo it on the February 28. I had it in the hood, and instead it should have been on the bench with a watch glass over it.



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