User:Melissa Novy/Notebook/CHEM-572/2013/02/13

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(Objectives)
Line 18: Line 18:
* Make a calibration curve for the determination of Ag<sup>+</sup> in solutions.
* Make a calibration curve for the determination of Ag<sup>+</sup> in solutions.
** Make 0.10 M AgNO<sub>3</sub> solution.
** Make 0.10 M AgNO<sub>3</sub> solution.
 +
* Remove PLA2002D + 5 wt % LMT film from glass mold.
==0.1 M AgNO<sub>3</sub> Solution==
==0.1 M AgNO<sub>3</sub> Solution==

Revision as of 13:54, 13 February 2013

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Objectives

  • Make a calibration curve for the determination of Ag+ in solutions.
    • Make 0.10 M AgNO3 solution.
  • Remove PLA2002D + 5 wt % LMT film from glass mold.

0.1 M AgNO3 Solution

  • Calculations
  250 mL of 0.1 M AgNO3
  MW AgNO3 = 169.87 g/mol
  0.1 M × 0.250 L = 0.025 mol
  0.025 mol AgNO3 × (169.87 g AgNO3/1 mol AgNO3) = 4.24675 g AgNO3
  • Actual mass AgNO3: 4.24694 g
  • Actual molarity AgNO3: 0.10000 M AgNO3

Ag+ Ion Selective Electrode Calibration

  • The protocol from 2013/02/12 was followed using solutions of the following [AgNO3]:
    • 0 M AgNO3
    • 0.0001 M AgNO3
    • 0.0010 M AgNO3
    • 0.0105 M AgNO3
    • 0.1000M AgNO3
  • Conductivity of solutions of AgNO3
[Ag+] [M] log [Ag+] [] Conductivity [mV]
0.000000394.6
0.000000390.7
0.000000386.4
0.00010-4377
0.00010-4375.2
0.00010-4374.7
0.00100-3411.6
0.00100-3411.8
0.00100-3411.8
0.01050-1.98470.1
0.01050-1.98470.3
0.01050-1.98470.3
0.10000-1528.5
0.10000-1528.5
0.10000-1528.5



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