User:Michael S. Bible/Notebook/581/2014/09/05: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
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==Notes==
==Notes==


I was sick today and unable to make it to lab.  My lab partners, Tami and Andrew, performed the FTIR and DSC in my absence.   
I was sick today and unable to make it to lab.  My lab partners, Tami and Andrew, performed the FTIR and DSC in my absence.  Although I was absent, I have created charts of the FTIR data gathered by my lab partners.


The Figure 0.1 below shows the FTIR data for the polymer-only samples that were soaked in MG solutions.  The Figure 0.2 is a close-up view of the region of the FTIR graph that presented the most separation between sample readings. 
Figure 0.1
<br>[[Image:FTIR_for_Polymer_Without_Clay_Additions.png|1000px]]
Figure 0.2
<br>[[Image:FTIR_Polymer_without_clay_Close_up.png|1000px]]
The Figure 0.3 below shows the FTIR data for the polymer + clay samples that were soaked in MG solutions.  The Figure 0.4 is a close-up view of the region of the FTIR graph that presented the most separation between sample readings.
Figure 0.3
<br>[[Image:FTIR_Polymer_With_Clay.png|1000px]]
Figure 0.4
<br>[[Image:FTIR_Polymer_With_Clay_Close_up.png|1000px]]
====Analysis of Differential Scanning Calorimetry Data====
Data below was taken from [[User:Tamanika_Tinsley/Notebook/Chem_581_Biomaterials_Design_Lab/2014/09/12|Tami's Notebook]].
The following figures show the Differential Scanning Results for the PVA with clay at different concentrations of malachite green.(See Figures 1-5)
Figure 1. PVA with Clay
<br>[[Image:pva with clay dsc.png]]
Figure 2. Clay at 2ppm
<br>[[Image:2ppm clay dsc.png]]
Figure 3. Clay at 8ppm
<br>[[Image:8ppm clay dsc.png]]
Figure 4. Clay at 80ppm
<br>[[Image:80ppm clay dsc.png]]
Figure 5. Clay at 200ppm
<br>[[Image:200ppm clay dsc.png]]
The following figures show the Differential Scanning Results for the PVA at different concentrations of malachite green.(See Figures 6-10)
Figure 6. PVA
<br>[[Image:PVA dsc.png]]
Figure 7. PVA at 2ppm
<br>[[Image:PVA 2ppm dsc.png]]
Figure 8. PVA at 8ppm
<br>[[Image:PVA 8ppm dsc.png]]
Figure 9. PVA at 80ppm
<br>[[Image:PVA 80ppm dsc.png]]
Figure 10. PVA at 200ppm
<br>[[Image:PVA 200ppm dsc.png]]


[[Category:Course]]
[[Category:Course]]

Latest revision as of 00:18, 27 September 2017

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Objective

Perform FTIR and DSC on the film samples that were soaked in MG solutions.

Description

I was sick today, so what was done can be found in Tami's notebook.

Data

Figure 1. Shows the weights of the pans, lids and films used for DSC

Notes

I was sick today and unable to make it to lab. My lab partners, Tami and Andrew, performed the FTIR and DSC in my absence. Although I was absent, I have created charts of the FTIR data gathered by my lab partners.

The Figure 0.1 below shows the FTIR data for the polymer-only samples that were soaked in MG solutions. The Figure 0.2 is a close-up view of the region of the FTIR graph that presented the most separation between sample readings.

Figure 0.1

Figure 0.2


The Figure 0.3 below shows the FTIR data for the polymer + clay samples that were soaked in MG solutions. The Figure 0.4 is a close-up view of the region of the FTIR graph that presented the most separation between sample readings.

Figure 0.3

Figure 0.4


Analysis of Differential Scanning Calorimetry Data

Data below was taken from Tami's Notebook.

The following figures show the Differential Scanning Results for the PVA with clay at different concentrations of malachite green.(See Figures 1-5)

Figure 1. PVA with Clay

Figure 2. Clay at 2ppm

Figure 3. Clay at 8ppm

Figure 4. Clay at 80ppm

Figure 5. Clay at 200ppm

The following figures show the Differential Scanning Results for the PVA at different concentrations of malachite green.(See Figures 6-10)

Figure 6. PVA

Figure 7. PVA at 2ppm

Figure 8. PVA at 8ppm

Figure 9. PVA at 80ppm

Figure 10. PVA at 200ppm