User:Mobeen Ashraf/Notebook/Chem-581/2012/11/20

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==Objective==
==Objective==
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Objective 1) Swelling Studies of PVOH Film with a molar mass of MW=22,000 g/mol.
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Objective 1) Swelling Studies of PVOH film with 1ml glutaraldehyde with a molar mass of MW=22,000 g/mol.
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Objective 2) 5-(4,6-dichlorotriazinyl)aminofluoresceine (5-DTFA)Dye Attachment.
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Objective 2) 5 - (4,6-dichlorotriazinyl) aminofluoresceine (5-DTFA) Dye Attachment studies.
==Description==
==Description==
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* Swelling Studies:
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** mass of PVOH film with 1 ml glutaraldehyde = 0.6707g. Note: The film was dried effectively before it was weigh.
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* 3 PVOH films were prepared: 0.5 g MW of 22,000, 1 ml glutaraldehyde, and 1 ml of porphrine dihydrogen chloride.
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* AAS studies for all the Cu standards: NaMT- concentration of 1.25 g/500 ml, for 1min, 5 min and 10 mins standards, 50 % CEC exchange-concentration of 1.25 g/500 ml, for 1 min, 5 min and 10 mins standards, 100% CEC exchange, for 1 min, 5 min and 10 mins standards, and Fe3O4-concentration of 1.25 g/500 ml, for 1 min, 5 min and 10 mins standards.
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* Dye Attachment
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** mass of PVOH = 0.500 g was placed in a small, 10 ml beaker
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** MW of PVOH = 22,000 g/mol
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** PVOH was then dissolved in 8 mL of 0.1M NaHCO3 (sodium bicarbonate) buffered solution (at a pH of around 10) for successful deprotination of the dye.  
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** The entire solution was then heated and stirred at until all of the dye was dissolved
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** After that about 1 mg of the dye was added to the resultant solution
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** The entire solution was heated up to 1 hour
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** Finally, the solution was poured into the big teflon plate and was stored for about 1 week.
==Data==
==Data==

Current revision

Experimental Chemistry Main project page
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Objective

Objective 1) Swelling Studies of PVOH film with 1ml glutaraldehyde with a molar mass of MW=22,000 g/mol.

Objective 2) 5 - (4,6-dichlorotriazinyl) aminofluoresceine (5-DTFA) Dye Attachment studies.

Description

  • Swelling Studies:
    • mass of PVOH film with 1 ml glutaraldehyde = 0.6707g. Note: The film was dried effectively before it was weigh.


  • Dye Attachment
    • mass of PVOH = 0.500 g was placed in a small, 10 ml beaker
    • MW of PVOH = 22,000 g/mol
    • PVOH was then dissolved in 8 mL of 0.1M NaHCO3 (sodium bicarbonate) buffered solution (at a pH of around 10) for successful deprotination of the dye.
    • The entire solution was then heated and stirred at until all of the dye was dissolved
    • After that about 1 mg of the dye was added to the resultant solution
    • The entire solution was heated up to 1 hour
    • Finally, the solution was poured into the big teflon plate and was stored for about 1 week.

Data

  • Add data and results here...

Notes

This area is for any observations or conclusions that you would like to note.


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.



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