User:Moira M. Esson/Notebook/CHEM-571/2014/04/16

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(Objectives)
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==Objectives==
 
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#AA
 
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#DSC
 
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#Microscope
 
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<br>
 
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==Microscope==
 
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*Please refer to Puja Mody's notebook for all microscope data
 
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<br>
 
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==Atomic Absorption==
 
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*AA was used to analyze the presence of both iron and gold for all remaining samples
 
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<br>
 
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Figure 1. Calibration curve for iron standards
 
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[[Image:Calibration curve of gold standards for atomic absorption analysis of biomineralized proteins with gold and magnetite nanoparticles correct .png|500px]]
 
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<br>
 
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Figure 2. Calibration curve for gold standards
 
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[[Image:Calibration curve of gold standards for atomic absorption analysis of biomineralized proteins with gold and magnetite nanoparticles correct.png|500px]]
 
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<br>
 
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Table 1. Iron Atomic Absorption Analysis of samples
 
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<br>
 
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{| {{table}}
 
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| align="center" style="background:#f0f0f0;"|'''Sample name'''
 
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| align="center" style="background:#f0f0f0;"|'''Concentration Iron in sample (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Total concentration Iron originally in solution (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Concentration Iron incorporated (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Percent Iron incorporated (%)'''
 
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|-
 
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| 13500:1 Mag:BSA N2 prep||0.022256152||1765.35||1765.327744||99.99873928
 
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|-
 
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| 13500:1 Mag:BSA N2 prep with Au||0.022219961||1765.35||1765.32778||99.99874133
 
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|-
 
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| 13000:1 Mag:BSA oven||0.02224606||1765.35||1765.327754||99.99873985
 
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|-
 
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| 16500:1 Mag:Heme oven||0.02224084||1765.35||1765.327759||99.99874015
 
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|-
 
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| 16500:1 Mag:Heme:Au oven||0.022238231||1765.35||1765.327762||99.99874029
 
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|-
 
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| 16500:1 Mag:Heme:Au sonicated||0.022220831||1765.35||1765.327779||99.99874128
 
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|-
 
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| 13500:1 Mag:BSA:Au sonicated||0.022207781||1765.35||1765.327792||99.99874202
 
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|-
 
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| 13000:1 Mag:BSA:Au oven||0.022180812||1765.35||1765.327819||99.99874355
 
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|}
 
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<br>
 
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Table 2.Gold atomic absorption analysis of samples
 
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{| {{table}}
 
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| align="center" style="background:#f0f0f0;"|'''Sample name'''
 
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| align="center" style="background:#f0f0f0;"|'''Concentration Gold in sample (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Total concentration Gold originally in solution (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Concentration gold incorporated (ug/mL)'''
 
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| align="center" style="background:#f0f0f0;"|'''Percent Gold incorporated (%)'''
 
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|-
 
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| 13500:1 Mag:BSA N2 prep with Au||0.04467344||49.2425||49.19782656||99.90927869
 
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|-
 
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| 13500:1 Mag:BSA:Au sonicated||0.0464768||49.2425||49.1960232||99.90561649
 
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|-
 
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| 13000:1 Mag:BSA:Au oven||0.04685952||49.2425||49.19564048||99.90483928
 
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|-
 
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| 16500:1 Mag:Heme:Au oven||0.04447792||49.2425||49.19802208||99.90967575
 
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|-
 
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| 16500:1 Mag:Heme:Au sonicated||0.04400784||49.2425||49.19849216||99.91063037
 
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|}
 
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<br>
 
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