User:Moira M. Esson/Notebook/CHEM-581/2012/10/10 - Revision history

Moira M. Esson: /* Atomic Absorption */

Moira M. Esson — Tue, 16 Oct 2012 14:01:56 GMT

Atomic Absorption

←Older revision		Revision as of 14:01, 16 October 2012
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	==Atomic Absorption==		==Atomic Absorption==
	*Solutions run were prepared on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/21\|2012/09/21]]		*Solutions run were prepared on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/21\|2012/09/21]]
-	*The General Protocol for AA described on [[User:Moira_M._Esson/Notebook/~~Chem~~-581/2012/10/05\|2012/10/05]] was used	+	*The General Protocol for AA described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/10/05\|2012/10/05]] was used
	<br>		<br>
	'''Atomic Absorption Data from AA wizard''':		'''Atomic Absorption Data from AA wizard''':

Moira M. Esson: /* DSC */

Moira M. Esson — Tue, 16 Oct 2012 14:01:41 GMT

DSC

←Older revision		Revision as of 14:01, 16 October 2012
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	==DSC==		==DSC==
-	Samples were prepared following the general protocol for DSC preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/07\|2012/9/07]]	+	Samples were prepared following the general protocol for DSC preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/07\|2012/9/07]]
	<br>		<br>
	'''DSC Sample Preparation'''		'''DSC Sample Preparation'''
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	\|}		\|}
	*'''Note''':DSC did not have the attached gas and was unable to be used. Prepared samples will be run and the data will be collected when next in the labaratory		*'''Note''':DSC did not have the attached gas and was unable to be used. Prepared samples will be run and the data will be collected when next in the labaratory
		+
	==Atomic Absorption==		==Atomic Absorption==
	*Solutions run were prepared on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/21\|2012/09/21]]		*Solutions run were prepared on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/21\|2012/09/21]]

Moira M. Esson: /* Objectives */

Moira M. Esson — Tue, 16 Oct 2012 14:01:22 GMT

Objectives

←Older revision		Revision as of 14:01, 16 October 2012
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	==Objectives==		==Objectives==
	#Prepare samples for DSC		#Prepare samples for DSC
-	#Run clay exchange described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/26\|2012/9/26]] using Fe<sub>3</sub>O<sub>4</sub>	+	#Run clay exchange described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/26\|2012/09/26]] using Fe<sub>3</sub>O<sub>4</sub>
	#Rerun AA for CuSO<sub>4</sub> solutions		#Rerun AA for CuSO<sub>4</sub> solutions
		+
	==DSC==		==DSC==
	Samples were prepared following the general protocol for DSC preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/07\|2012/9/07]]		Samples were prepared following the general protocol for DSC preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/07\|2012/9/07]]

Moira M. Esson: /* Atomic Absorption */

Moira M. Esson — Mon, 15 Oct 2012 02:01:16 GMT

Atomic Absorption

←Older revision		Revision as of 02:01, 15 October 2012
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	\| UNK24\|\|10ppm CEC 50% 10min\|\|\|\|15.0057\|\|0.6102		\| UNK24\|\|10ppm CEC 50% 10min\|\|\|\|15.0057\|\|0.6102
	\|}		\|}
		+	<br>
		+	'''Calibration Curve'''

		+	'''General Notes''':
		+	*The standards used were too high of a concentration. Need to remake CuSO<sub>4</sub> standards between 5-20ppm.
		+	*All Fe<sub>3</sub>O<sub>4</sub> samples need to be reprepared and retested. Solutions were prepared with CuSO<sub>4</sub> instead of deionized H<sub>2</sub>O. Concentrations were inaccurate and calibration curve created was inaccurate
		+	*AA needs to be run again

	<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->

Moira M. Esson: /* Atomic Absorption */

Moira M. Esson — Mon, 15 Oct 2012 01:53:49 GMT

Atomic Absorption

←Older revision		Revision as of 01:53, 15 October 2012
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	*'''Note''':DSC did not have the attached gas and was unable to be used. Prepared samples will be run and the data will be collected when next in the labaratory		*'''Note''':DSC did not have the attached gas and was unable to be used. Prepared samples will be run and the data will be collected when next in the labaratory
	==Atomic Absorption==		==Atomic Absorption==
-	*Solutions run were prepared on	+	*Solutions run were prepared on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/21\|2012/09/21]]
		+	*The General Protocol for AA described on [[User:Moira_M._Esson/Notebook/Chem-581/2012/10/05\|2012/10/05]] was used
		+	<br>
		+	'''Atomic Absorption Data from AA wizard''':

	{\| {{table}}		{\| {{table}}

Moira M. Esson: /* DSC */

Moira M. Esson — Mon, 15 Oct 2012 01:49:54 GMT

DSC

←Older revision		Revision as of 01:49, 15 October 2012
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	#Rerun AA for CuSO<sub>4</sub> solutions		#Rerun AA for CuSO<sub>4</sub> solutions
	==DSC==		==DSC==
-	*Samples were prepared following the general protocol for DSC preparation	+	Samples were prepared following the general protocol for DSC preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/07\|2012/9/07]]
		+	<br>
		+	'''DSC Sample Preparation'''
		+	{\| {{table}}
		+	\| align="center" style="background:#f0f0f0;"\|'''Sample Name'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Pan+lid mass(g)'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Mass sample(g)'''
		+	\|-
		+	\| PVOH 130,000+[H3PO4]+15%maleic acid\|\|0.04939\|\|0.00281
		+	\|-
		+	\| PVOH 130,000\|\|0.0495\|\|0.00283
		+	\|-
		+	\| PVOH 22,000+[HCl]\|\|0.04933\|\|
		+	\|}
		+	*'''Note''':DSC did not have the attached gas and was unable to be used. Prepared samples will be run and the data will be collected when next in the labaratory
		+	==Atomic Absorption==
		+	*Solutions run were prepared on

	{\| {{table}}		{\| {{table}}

Moira M. Esson: /* Entry title */

Moira M. Esson — Mon, 15 Oct 2012 01:31:15 GMT

Entry title

←Older revision		Revision as of 01:31, 15 October 2012
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	\| colspan="2"\|		\| colspan="2"\|
	<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
-	==~~Entry title~~==	+	==Objectives==
		+	#Prepare samples for DSC
		+	#Run clay exchange described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/9/26\|2012/9/26]] using Fe<sub>3</sub>O<sub>4</sub>
		+	#Rerun AA for CuSO<sub>4</sub> solutions
		+	==DSC==
		+	*Samples were prepared following the general protocol for DSC preparation
		+
	{\| {{table}}		{\| {{table}}
	\| align="center" style="background:#f0f0f0;"\|'''Cu'''		\| align="center" style="background:#f0f0f0;"\|'''Cu'''

Moira M. Esson: /* Entry title */

Moira M. Esson — Thu, 11 Oct 2012 17:21:53 GMT

Entry title

←Older revision		Revision as of 17:21, 11 October 2012
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	<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
	==Entry title==		==Entry title==
-	* Insert content here...	+	{\| {{table}}
		+	\| align="center" style="background:#f0f0f0;"\|'''Cu'''
		+	\| align="center" style="background:#f0f0f0;"\|''''''
		+	\| align="center" style="background:#f0f0f0;"\|''''''
		+	\| align="center" style="background:#f0f0f0;"\|''''''
		+	\| align="center" style="background:#f0f0f0;"\|''''''
		+	\|-
		+	\| Action\|\|Sample ID\|\|True Value (ppm)\|\|Conc. (ppm)\|\|Abs.
		+	\|-
		+	\| AUTOZERO\|\|\|\|\|\|\|\|
		+	\|-
		+	\| STD\|\|STD 1 \|\|1\|\|\|\|0.0054
		+	\|-
		+	\| STD\|\|STD 2 \|\|5\|\|\|\|0.0118
		+	\|-
		+	\| STD\|\|STD 3 \|\|10\|\|\|\|0.6531
		+	\|-
		+	\| STD\|\|STD 4 \|\|20\|\|\|\|1.0516
		+	\|-
		+	\| STD\|\|STD 5 \|\|25\|\|\|\|1.1173
		+	\|-
		+	\| STD\|\|STD 6 \|\|30\|\|\|\|1.1773
		+	\|-
		+	\| STD\|\|STD 7 \|\|40\|\|\|\|1.2726
		+	\|-
		+	\| STD\|\|STD 8 \|\|50\|\|\|\|1.3179
		+	\|-
		+	\| UNK1\|\|7.4ppm NaMT 1min\|\|\|\|7.5551\|\|0.3993
		+	\|-
		+	\| UNK2\|\|10ppm NaMT 1 min\|\|\|\|10.9678\|\|0.4959
		+	\|-
		+	\| UNK3\|\|7.4ppm NaMT 5 min\|\|\|\|7.0393\|\|0.3847
		+	\|-
		+	\| UNK4\|\|10ppm NaMT 5 min\|\|\|\|10.6639\|\|0.4873
		+	\|-
		+	\| UNK5\|\|7.4ppm NaMt 10 min\|\|\|\|4.2696\|\|0.3063
		+	\|-
		+	\| UNK6\|\|10ppm NaMT 10min\|\|\|\|7.2478\|\|0.3906
		+	\|-
		+	\| UNK7\|\|7.4ppm Fe3O4 1min\|\|\|\|46.4402\|\|1.5
		+	\|-
		+	\| UNK8\|\|10ppm Fe3O4 1 min\|\|\|\|44.9883\|\|1.4589
		+	\|-
		+	\| UNK9\|\|7.4ppm Fe3O4 5min\|\|\|\|39.7598\|\|1.3109
		+	\|-
		+	\| UNK10\|\|10ppm Fe3O4 5min\|\|\|\|43.9567\|\|1.4297
		+	\|-
		+	\| UNK11\|\|7.4ppm Fe3O4 10min\|\|\|\|39.841\|\|1.3132
		+	\|-
		+	\| UNK12\|\|10ppm Fe3O4 10min\|\|\|\|39.9647\|\|1.3167
		+	\|-
		+	\| UNK13\|\|7.4ppm CEC100% 1min\|\|\|\|11.1939\|\|0.5023
		+	\|-
		+	\| UNK14\|\|10ppmCEC100% 1min\|\|\|\|16.5283\|\|0.6533
		+	\|-
		+	\| UNK15\|\|7.4ppm CEC100% 5min\|\|\|\|9.5123\|\|0.4547
		+	\|-
		+	\| UNK16\|\|10ppm CEC100% 5min\|\|\|\|15.4473\|\|0.6227
		+	\|-
		+	\| UNK17\|\|7.4ppm CEC100% 10min\|\|\|\|8.4171\|\|0.4237
		+	\|-
		+	\| UNK18\|\|10ppm CEC100% 10min\|\|\|\|15.7794\|\|0.6321
		+	\|-
		+	\| UNK19\|\|7.4ppm CEC 50% 1min\|\|\|\|10.5191\|\|0.4832
		+	\|-
		+	\| UNK20\|\|10ppm CEC 50% 1min\|\|\|\|14.7443\|\|0.6028
		+	\|-
		+	\| UNK21\|\|7.4ppm CEC 50% 5min\|\|\|\|9.802\|\|0.4629
		+	\|-
		+	\| UNK22\|\|10ppm CEC 50% 5min\|\|\|\|15.3449\|\|0.6198
		+	\|-
		+	\| UNK23\|\|7.4ppm CEC 50% 10min\|\|\|\|10.4449\|\|0.4811
		+	\|-
		+	\| UNK24\|\|10ppm CEC 50% 10min\|\|\|\|15.0057\|\|0.6102
		+	\|}

Moira M. Esson: Autocreate 2012/10/10 Entry for User:Moira_M._Esson/Notebook/CHEM-581

Moira M. Esson — Thu, 11 Oct 2012 17:21:08 GMT

Autocreate 2012/10/10 Entry for User:Moira_M._Esson/Notebook/CHEM-581

New page

{|{{table}} width="800"
|-
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>      </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|-
| colspan="2"|

==Entry title==
* Insert content here...


|}

__NOTOC__