User:Moira M. Esson/Notebook/CHEM-581/2012/10/19: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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Using the following concentrations(shown above), a calibration curve was prepared. | |||
<br> | |||
[[Image:Cu%2B2_AAS_Calibration_Curve.png]] | |||
==Crosslinking== | ==Crosslinking== | ||
*The general protocol for crosslinking glutaraldehyde films described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/14|2012/09/14]] was followed. | *The general protocol for crosslinking glutaraldehyde films described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/14|2012/09/14]] was followed. | ||
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*From the amount of leakage, it appears as if 0.5mL glutaraldehyde per 1g PVOH in a large Teflon dish is not sufficient. For next film preparation, 1mL of glutaraldehyde will be used | *From the amount of leakage, it appears as if 0.5mL glutaraldehyde per 1g PVOH in a large Teflon dish is not sufficient. For next film preparation, 1mL of glutaraldehyde will be used | ||
*approximately 12mL of each solution was saved after crosslinking | *approximately 12mL of each solution was saved after crosslinking | ||
==Fe<sub>3</sub>O<sub>4</sub>== | ==Fe<sub>3</sub>O<sub>4</sub> Filtrates== | ||
*It was observed that the Fe<sub>3</sub>O<sub>4</sub> filtrates all contained clay at the bottom of vial | *It was observed that the Fe<sub>3</sub>O<sub>4</sub> filtrates all contained clay at the bottom of vial | ||
*The general protocol for adsorption of clays described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/26|2012/09/26]] in CuSO<sub>4</sub> was used | *The general protocol for adsorption of clays described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/26|2012/09/26]] in CuSO<sub>4</sub> was used |
Latest revision as of 22:10, 26 September 2017
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Objectives
AA
AA Data collected:
Crosslinking
Crosslinking notes:
Fe3O4 Filtrates
Fe3O4 filtrate data
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