User:Moira M. Esson/Notebook/CHEM-581/2012/10/26: Difference between revisions
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*Film 1mLGA+HCl remained dark green and more stiff than other film. Turned pink after addition to deionized H<sub>2</sub>O | *Film 1mLGA+HCl remained dark green and more stiff than other film. Turned pink after addition to deionized H<sub>2</sub>O | ||
<br> | <br> | ||
Please refer to [[User:Karlena_L._Brown/Notebook/CHEM-581/2012/10/26]] and [[User:Melissa_Novy/Notebook/CHEM-581/2012/10/26]] for calculations relating to preparation of higher concentration of porphyrin solutions and salt. | Please refer to [[User:Karlena_L._Brown/Notebook/CHEM-581/2012/10/26]] and [[User:Melissa_Novy/Notebook/CHEM-581/2012/10/26]] for calculations relating to preparation of higher concentration of porphyrin solutions and salt. | ||
==AA== | |||
*Ran AA following the general protocol for atomic absorption. Ran on solutions collected from film adsorption completed [[User:Moira_M._Esson/Notebook/CHEM-581/2012/10/17|2012/10/17]] | |||
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*Atomic Absorption Data | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''''' | |||
| align="center" style="background:#f0f0f0;"|'''Concentration [ppm]''' | |||
| align="center" style="background:#f0f0f0;"|'''Abs. [ ]''' | |||
| align="center" style="background:#f0f0f0;"|'''BG''' | |||
| align="center" style="background:#f0f0f0;"|'''''' | |||
|- | |||
| ||0.01||-0.00600||0.00200|| | |||
|- | |||
| ||0.05||-0.01160||0.00540|| | |||
|- | |||
| ||1||-0.00920||0.00150|| | |||
|- | |||
| ||2||0.11710||0.00470|| | |||
|- | |||
| ||3||0.20330||0.00330|| | |||
|- | |||
| ||Given Conc. [ppm]||Abs. [ ]||BG||Conc. [ppm] | |||
|- | |||
| 1 min NaMT-CuSO<sub>4</sub>||7.4||0.37690||0.00430||5.63990 | |||
|- | |||
| ||10||0.47600||0.00620||7.01910 | |||
|- | |||
| 5 min NaMT-CuSO<sub>4</sub>||7.4||0.38080||0.00350||5.69420 | |||
|- | |||
| ||10||0.48150||0.00600||7.09560 | |||
|- | |||
| 10 min NaMT-CuSO<sub>4</sub>||7.4||0.29540||0.00370||4.50580 | |||
|- | |||
| ||10||0.37640||0.00480||5.63300 | |||
|- | |||
| 1 min 100%CEC NaMT-CuSO<sub>4</sub>||7.4||0.48030||0.00680||7.07890 | |||
|- | |||
| ||10||0.61880||0.00950||9.00630 | |||
|- | |||
| 5 min 100%CEC NaMT-CuSO<sub>4</sub>||7.4||0.46120||0.00640||6.81310 | |||
|- | |||
| ||10||0.62080||0.00790||9.03420 | |||
|- | |||
| 10 min 100%CEC NaMT-CuSO<sub>4</sub>||7.4||0.43300||0.00400||6.42070 | |||
|- | |||
| ||10||0.62960||0.00480||9.15660 | |||
|- | |||
| 1 min 50%CEC NaMT-CuSO<sub>4</sub>||7.4||0.47470||0.00530||7.00100 | |||
|- | |||
| ||10||0.62050||0.00490||9.03000 | |||
|- | |||
| 5 min 50%CEC NaMT-CuSO<sub>4</sub>||7.4||0.46110||0.00310||6.81170 | |||
|- | |||
| ||10||0.60940||0.00580||8.87550 | |||
|- | |||
| 10 min 50%CEC NaMT-CuSO<sub>4</sub>||7.4||0.46800||0.00390||6.90770 | |||
|- | |||
| ||10||0.59620||0.00440||8.69180 | |||
|} | |||
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Revision as of 12:22, 30 November 2012
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Objectives
Crosslinking
Crosslinked Films:
Observations for crosslinking films
AA
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