User:Moira M. Esson/Notebook/CHEM-581/2013/04/12: Difference between revisions
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# Close the door to the x-ray | # Close the door to the x-ray | ||
# Open software on computer | # Open software on computer | ||
*50:50 PVA 130K:110%LP was run on the x-ray. The data will be collected during the next session. | *50:50 PVA 130K:110%LP was run on the x-ray. The data will be collected during the next session. | ||
==Hydrogel DSC preparation== | ==Hydrogel DSC preparation== | ||
*3mL of deionized H<sub>2</sub>O was added to each of the hydrogel samples. H<sub>2</sub>O was added in order to soften the hydrogels to allow DSC sample preparation. H<sub>2</sub>O was also added in order to remove any excess Rhodamine 6G still present. | *3mL of deionized H<sub>2</sub>O was added to each of the hydrogel samples. H<sub>2</sub>O was added in order to soften the hydrogels to allow DSC sample preparation. H<sub>2</sub>O was also added in order to remove any excess Rhodamine 6G still present. |
Revision as of 10:19, 15 April 2013
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Objectives
DSC
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again
Film Preparation
X-Ray AnalysisGeneral Protocol:
Hydrogel DSC preparation
MicroscopeNotes
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