User:Moira M. Esson/Notebook/CHEM-581/2013/04/19: Difference between revisions
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==X-ray== | ==X-ray== | ||
General Protocol: | |||
# Use a Kimwipe and acetone to thoroughly clean the low background sample holder | |||
# Insert Sample into the low background holder. Note: Must make sure that the sample is completely flat and that the particle sample size is very small. If the sample is too large, use a mortar and pestle to completely grind the sample | |||
# Turn on the chiller | |||
# Turn on Miniflex II. This is the white button on the machine | |||
# Turn on X-ray. The machine will be on when the red lights on the button labeled x-ray light up | |||
# Using a Geiger counter, test the radiation from the machine | |||
# Set sample in sample holder and record sample holder number | |||
# Close the door to the x-ray | |||
# Open software on computer | |||
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*The samples will be posted when received. | |||
Revision as of 15:43, 23 April 2013
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Objectives
Pressure Testing
Figure 1. Pressure testing of prepared microspheres.
X-rayGeneral Protocol:
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