User:NYOUSHA Yousefi/Notebook/Protein Engineering/2012/10/16

From OpenWetWare

(Difference between revisions)
Jump to: navigation, search
(Objectives)
(Objective2)
Line 13: Line 13:
==Objective2==
==Objective2==
 +
The chromium protoporphyrin IX reaction, which was allowed to run for a week, was filtered.
==Procedure1==   
==Procedure1==   

Revision as of 14:02, 16 October 2012

Project name Main project page
Previous entry      Next entry

Entry title

Zinc protoporphyrin IX synthesis

Objective1

The Zinc Protoporphyrin IX produced in previous labs was not pure enough for further studies, therefore it was synthesized again. The values of the reactants were doubled to force the reaction toward the products and completion.

Objective2

The chromium protoporphyrin IX reaction, which was allowed to run for a week, was filtered.

Procedure1

  1. 20ml of DMF (solvent) was brought to boiling point under a condenser.
  2. 0.2009g of protoporphyrin IX was added to the solvent and the mixture was allowed to boil for 20min.
  3. 0.0458g of zinc acetate was added to the boiling mixture and the reaction was allowed to run over the night.

Procedure2


Personal tools