|
|
| (4 intermediate revisions not shown.) |
| Line 16: |
Line 16: |
| | *Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence. | | *Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence. |
| | | | |
| - | Table 1: UV-VIS Results
| + | [[Image:Absorbance of UV-Vis Graph.JPG]] |
| - | | + | |
| - | *Wavelength nm. Absorbance (DMF) 4um 2um 0.5um
| + | |
| - | *200 0.002 4.323 4.798 4.798
| + | |
| - | *201 0.002 4.798 4.798 4.798
| + | |
| - | *202 0.003 4.798 4.798 4.323
| + | |
| - | *203 0.002 4.798 4.798 4.798
| + | |
| - | *204 0.001 4.798 5 4.798
| + | |
| - | *205 0.002 4.798 4.798 4.798
| + | |
| - | *206 0.001 5 4.798 4.798
| + | |
| - | *207 0.001 5 5 5
| + | |
| - | *208 0.001 4.798 4.798 4.798
| + | |
| - | *209 0 5 5 5
| + | |
| - | *210 0.001 5 5 5
| + | |
| - | *211 0 5 5 5
| + | |
| - | *212 0 5 5 5
| + | |
| - | *213 -0.001 5 5 5
| + | |
| - | *214 -0.001 5 5 5
| + | |
| - | *215 -0.001 5 5 5
| + | |
| - | *216 -0.001 5 5 5
| + | |
| - | *217 -0.001 5 5 5
| + | |
| - | *218 -0.001 5 5 5
| + | |
| - | *219 0 5 5 5
| + | |
| - | *220 -0.001 5 5 5
| + | |
| - | *221 -0.001 5 5 5
| + | |
| - | *222 -0.001 5 5 5
| + | |
| - | *223 -0.001 5 5 5
| + | |
| - | *224 -0.001 5 5 5
| + | |
| - | *225 -0.001 5 5 5
| + | |
| - | *226 -0.001 5 5 5
| + | |
| - | *227 -0.001 5 5 5
| + | |
| - | *228 -0.001 5 5 5
| + | |
| - | *229 -0.001 5 5 5
| + | |
| - | *230 -0.001 5 5 5
| + | |
| - | *231 -0.001 5 5 5
| + | |
| - | *232 -0.001 5 5 5
| + | |
| - | *233 -0.001 5 5 5
| + | |
| - | *234 -0.001 5 5 5
| + | |
| - | *235 -0.001 5 5 5
| + | |
| - | *236 -0.001 5 5 5
| + | |
| - | *237 -0.001 5 5 5
| + | |
| - | *238 -0.001 5 5 5
| + | |
| - | *239 -0.001 5 5 5
| + | |
| - | *240 -0.001 5 5 5
| + | |
| - | *241 -0.001 5 5 5
| + | |
| - | *242 -0.001 5 5 5
| + | |
| - | *243 -0.001 5 5 5
| + | |
| - | *244 -0.001 5 5 5
| + | |
| - | *245 -0.001 5 5 5
| + | |
| - | *246 -0.001 5 5 5
| + | |
| - | *247 -0.001 5 5 5
| + | |
| - | *248 -0.001 5 5 5
| + | |
| - | *249 -0.001 5 5 5
| + | |
| - | *250 -0.001 5 5 4.798
| + | |
| - | *251 -0.001 5 5 4.798
| + | |
| - | *252 -0.001 5 5 5
| + | |
| - | *253 -0.001 5 5 5
| + | |
| - | *254 -0.001 5 5 5
| + | |
| - | *255 -0.001 5 5 5
| + | |
| - | *256 -0.001 5 5 5
| + | |
| - | *257 -0.001 5 5 4.798
| + | |
| - | *258 -0.001 5 5 5
| + | |
| - | *259 -0.001 4.798 5 5
| + | |
| - | *260 -0.001 4.798 4.798 4.798
| + | |
| - | *261 -0.001 4.798 4.798 5
| + | |
| - | *262 -0.001 3.848 4.323 4.323
| + | |
| - | *263 -0.001 2.979 3.525 3.688
| + | |
| - | *264 -0.001 2.24 2.699 2.819
| + | |
| - | *265 0 1.659 2.002 2.095
| + | |
| - | *266 -0.001 1.246 1.494 1.569
| + | |
| - | *267 -0.001 0.937 1.121 1.17
| + | |
| - | *268 -0.001 0.715 0.844 0.878
| + | |
| - | *269 -0.001 0.567 0.66 0.687
| + | |
| - | *270 -0.001 0.463 0.534 0.555
| + | |
| - | *271 -0.001 0.391 0.443 0.457
| + | |
| - | *272 0 0.34 0.378 0.388
| + | |
| - | *273 0 0.304 0.332 0.34
| + | |
| - | *274 0 0.278 0.302 0.307
| + | |
| - | *275 -0.001 0.259 0.279 0.283
| + | |
| - | *276 -0.001 0.243 0.26 0.264
| + | |
| - | *277 -0.002 0.231 0.246 0.249
| + | |
| - | *278 -0.002 0.222 0.235 0.237
| + | |
| - | *279 -0.001 0.213 0.226 0.227
| + | |
| - | *280 0 0.207 0.217 0.219
| + | |
| - | *281 -0.001 0.2 0.209 0.211
| + | |
| - | *282 0 0.194 0.202 0.204
| + | |
| - | *283 0 0.188 0.195 0.197
| + | |
| - | *284 -0.001 0.183 0.189 0.19
| + | |
| - | *285 -0.001 0.177 0.183 0.184
| + | |
| - | *286 -0.001 0.173 0.178 0.179
| + | |
| - | *287 -0.001 0.167 0.173 0.173
| + | |
| - | *288 0 0.163 0.167 0.167
| + | |
| - | *289 -0.001 0.158 0.161 0.162
| + | |
| - | *290 -0.001 0.152 0.155 0.156
| + | |
| - | *291 -0.002 0.147 0.15 0.15
| + | |
| - | *292 -0.001 0.142 0.145 0.144
| + | |
| - | *293 -0.001 0.138 0.139 0.139
| + | |
| - | *294 -0.001 0.133 0.134 0.134
| + | |
| - | *295 -0.001 0.129 0.13 0.13
| + | |
| - | *296 -0.001 0.125 0.126 0.126
| + | |
| - | *297 -0.001 0.122 0.121 0.121
| + | |
| - | *298 -0.001 0.118 0.117 0.117
| + | |
| - | *299 -0.001 0.113 0.113 0.113
| + | |
| - | *300 -0.001 0.111 0.109 0.109
| + | |
| - | *301 -0.001 0.107 0.106 0.106
| + | |
| - | *302 0 0.106 0.102 0.103
| + | |
| - | *303 0 0.103 0.1 0.1
| + | |
| - | *304 -0.001 0.1 0.097 0.096
| + | |
| - | *305 -0.001 0.097 0.093 0.093
| + | |
| - | *306 -0.001 0.094 0.091 0.091
| + | |
| - | *307 -0.001 0.091 0.089 0.087
| + | |
| - | *308 -0.001 0.089 0.086 0.085
| + | |
| - | *309 0 0.087 0.083 0.082
| + | |
| - | *310 -0.001 0.085 0.08 0.079
| + | |
| - | *311 0 0.083 0.079 0.077
| + | |
| - | *312 -0.001 0.081 0.076 0.076
| + | |
| - | 313 0 0.08 0.075 0.073
| + | |
| - | 314 0 0.079 0.073 0.072
| + | |
| - | 315 -0.001 0.077 0.071 0.07
| + | |
| - | 316 -0.001 0.076 0.07 0.068
| + | |
| - | 317 0 0.075 0.068 0.067
| + | |
| - | 318 -0.001 0.074 0.068 0.066
| + | |
| - | 319 -0.001 0.073 0.066 0.064
| + | |
| - | 320 -0.001 0.072 0.065 0.063
| + | |
| - | 321 -0.001 0.071 0.064 0.063
| + | |
| - | 322 -0.001 0.07 0.062 0.061
| + | |
| - | 323 -0.001 0.07 0.062 0.06
| + | |
| - | 324 -0.001 0.069 0.061 0.059
| + | |
| - | 325 -0.001 0.069 0.061 0.058
| + | |
| - | 326 0 0.068 0.06 0.056
| + | |
| - | 327 -0.001 0.068 0.059 0.056
| + | |
| - | 328 -0.001 0.068 0.059 0.056
| + | |
| - | 329 0 0.067 0.058 0.054
| + | |
| - | 330 -0.001 0.067 0.058 0.054
| + | |
| - | 331 -0.001 0.067 0.056 0.053
| + | |
| - | 332 -0.001 0.067 0.057 0.052
| + | |
| - | 333 -0.001 0.067 0.057 0.053
| + | |
| - | 334 -0.001 0.066 0.055 0.052
| + | |
| - | 335 -0.001 0.066 0.055 0.051
| + | |
| - | 336 -0.001 0.066 0.056 0.052
| + | |
| - | 337 -0.001 0.067 0.055 0.05
| + | |
| - | 338 -0.001 0.067 0.054 0.05
| + | |
| - | 339 -0.001 0.067 0.055 0.049
| + | |
| - | 340 -0.002 0.065 0.053 0.048
| + | |
| - | 341 -0.001 0.067 0.054 0.048
| + | |
| - | 342 -0.001 0.066 0.053 0.048
| + | |
| - | 343 0 0.067 0.054 0.049
| + | |
| - | 344 0 0.067 0.053 0.048
| + | |
| - | 345 -0.001 0.067 0.054 0.047
| + | |
| - | 346 -0.001 0.067 0.053 0.047
| + | |
| - | 347 0 0.067 0.054 0.046
| + | |
| - | 348 -0.001 0.067 0.053 0.046
| + | |
| - | 349 -0.001 0.067 0.052 0.046
| + | |
| - | 350 -0.001 0.069 0.053 0.046
| + | |
| - | 351 0 0.068 0.053 0.046
| + | |
| - | 352 0 0.07 0.053 0.044
| + | |
| - | 353 0 0.07 0.053 0.045
| + | |
| - | 354 -0.001 0.07 0.054 0.045
| + | |
| - | 355 -0.002 0.072 0.054 0.044
| + | |
| - | 356 0 0.073 0.054 0.044
| + | |
| - | 357 0 0.074 0.055 0.044
| + | |
| - | 358 -0.001 0.075 0.054 0.043
| + | |
| - | 359 -0.001 0.075 0.056 0.043
| + | |
| - | 360 0.001 0.077 0.057 0.046
| + | |
| - | 361 -0.001 0.076 0.055 0.042
| + | |
| - | 362 0 0.077 0.055 0.042
| + | |
| - | 363 -0.001 0.078 0.055 0.042
| + | |
| - | 364 -0.001 0.079 0.055 0.042
| + | |
| - | 365 -0.001 0.08 0.056 0.041
| + | |
| - | 366 0 0.082 0.057 0.041
| + | |
| - | 367 0 0.084 0.058 0.042
| + | |
| - | 368 0 0.086 0.059 0.042
| + | |
| - | 369 0 0.087 0.06 0.042
| + | |
| - | 370 -0.001 0.089 0.06 0.042
| + | |
| - | 371 -0.001 0.091 0.061 0.041
| + | |
| - | 372 -0.001 0.093 0.062 0.042
| + | |
| - | 373 -0.001 0.096 0.063 0.042
| + | |
| - | 374 0 0.099 0.065 0.042
| + | |
| - | 375 -0.001 0.102 0.067 0.044
| + | |
| - | 376 -0.001 0.104 0.067 0.044
| + | |
| - | 377 0 0.107 0.069 0.044
| + | |
| - | 378 0 0.11 0.071 0.044
| + | |
| - | 379 0 0.112 0.072 0.044
| + | |
| - | 380 0 0.115 0.074 0.044
| + | |
| - | 381 -0.001 0.118 0.074 0.045
| + | |
| - | 382 0 0.12 0.076 0.045
| + | |
| - | 383 0 0.123 0.077 0.045
| + | |
| - | 384 0 0.125 0.078 0.044
| + | |
| - | 385 0 0.127 0.079 0.044
| + | |
| - | 386 0 0.13 0.08 0.044
| + | |
| - | 387 0 0.132 0.082 0.044
| + | |
| - | 388 -0.001 0.135 0.082 0.044
| + | |
| - | 389 -0.001 0.137 0.084 0.044
| + | |
| - | 390 -0.001 0.141 0.086 0.044
| + | |
| - | 391 -0.001 0.145 0.087 0.045
| + | |
| - | 392 0 0.148 0.09 0.045
| + | |
| - | 393 0 0.152 0.091 0.045
| + | |
| - | 394 -0.001 0.155 0.093 0.046
| + | |
| - | 395 0 0.16 0.095 0.046
| + | |
| - | 396 0 0.164 0.097 0.047
| + | |
| - | 397 0 0.167 0.099 0.047
| + | |
| - | 398 0 0.17 0.101 0.048
| + | |
| - | 399 0.001 0.174 0.103 0.048
| + | |
| - | 400 0 0.177 0.104 0.049
| + | |
| - | 401 0 0.18 0.106 0.049
| + | |
| - | 402 0 0.182 0.107 0.049
| + | |
| - | 403 0 0.183 0.108 0.049
| + | |
| - | 404 0 0.184 0.109 0.049
| + | |
| - | 405 0 0.183 0.108 0.049
| + | |
| - | 406 0 0.184 0.108 0.049
| + | |
| - | 407 0 0.182 0.107 0.049
| + | |
| - | 408 0 0.181 0.106 0.049
| + | |
| - | 409 0 0.178 0.105 0.049
| + | |
| - | 410 0 0.173 0.103 0.048
| + | |
| - | 411 0 0.17 0.101 0.048
| + | |
| - | 412 0 0.166 0.098 0.047
| + | |
| - | 413 0 0.161 0.095 0.047
| + | |
| - | 414 0 0.155 0.093 0.047
| + | |
| - | 415 0 0.15 0.09 0.046
| + | |
| - | 416 0 0.144 0.087 0.045
| + | |
| - | 417 0.001 0.138 0.084 0.044
| + | |
| - | 418 0.001 0.132 0.08 0.044
| + | |
| - | 419 0 0.126 0.077 0.043
| + | |
| - | 420 -0.001 0.12 0.073 0.041
| + | |
| - | 421 0.001 0.112 0.069 0.041
| + | |
| - | 422 0.001 0.106 0.066 0.039
| + | |
| - | 423 0.001 0.1 0.063 0.039
| + | |
| - | 424 0 0.094 0.059 0.038
| + | |
| - | 425 0 0.087 0.057 0.037
| + | |
| - | 426 -0.001 0.081 0.054 0.036
| + | |
| - | 427 0 0.076 0.051 0.035
| + | |
| - | 428 -0.001 0.071 0.049 0.034
| + | |
| - | 429 0 0.067 0.046 0.033
| + | |
| - | 430 -0.001 0.063 0.044 0.033
| + | |
| - | 431 0 0.06 0.043 0.032
| + | |
| - | 432 0 0.057 0.042 0.032
| + | |
| - | 433 0 0.055 0.04 0.031
| + | |
| - | 434 0 0.052 0.039 0.031
| + | |
| - | 435 0 0.05 0.038 0.031
| + | |
| - | 436 -0.001 0.048 0.037 0.031
| + | |
| - | 437 0 0.046 0.036 0.03
| + | |
| - | 438 -0.001 0.045 0.035 0.03
| + | |
| - | 439 -0.001 0.043 0.034 0.029
| + | |
| - | 440 0 0.042 0.034 0.029
| + | |
| - | 441 0.001 0.041 0.033 0.03
| + | |
| - | 442 0 0.04 0.032 0.03
| + | |
| - | 443 0 0.039 0.032 0.029
| + | |
| - | 444 0 0.038 0.032 0.029
| + | |
| - | 445 0 0.037 0.031 0.029
| + | |
| - | 446 0 0.037 0.031 0.029
| + | |
| - | 447 0 0.036 0.03 0.029
| + | |
| - | 448 0 0.036 0.031 0.029
| + | |
| - | 449 -0.001 0.035 0.03 0.029
| + | |
| - | 450 0 0.034 0.03 0.028
| + | |
| - | 451 0.001 0.035 0.03 0.029
| + | |
| - | 452 0 0.035 0.03 0.03
| + | |
| - | 453 0 0.034 0.03 0.029
| + | |
| - | 454 -0.001 0.034 0.03 0.03
| + | |
| - | 455 0 0.034 0.03 0.029
| + | |
| - | 456 0 0.034 0.03 0.029
| + | |
| - | 457 0 0.033 0.029 0.029
| + | |
| - | 458 0 0.032 0.029 0.029
| + | |
| - | 459 0.001 0.033 0.029 0.03
| + | |
| - | 460 0 0.033 0.03 0.03
| + | |
| - | 461 0 0.032 0.029 0.029
| + | |
| - | 462 0 0.032 0.029 0.029
| + | |
| - | 463 0 0.032 0.029 0.029
| + | |
| - | 464 0 0.032 0.029 0.029
| + | |
| - | 465 0 0.032 0.028 0.028
| + | |
| - | 466 0 0.032 0.028 0.028
| + | |
| - | 467 0 0.031 0.028 0.028
| + | |
| - | 468 0 0.031 0.028 0.028
| + | |
| - | 469 0 0.031 0.028 0.028
| + | |
| - | 470 0 0.031 0.028 0.028
| + | |
| - | 471 0 0.031 0.028 0.028
| + | |
| - | 472 0.001 0.032 0.028 0.029
| + | |
| - | 473 0 0.031 0.028 0.028
| + | |
| - | 474 0 0.031 0.028 0.028
| + | |
| - | 475 0 0.032 0.028 0.028
| + | |
| - | 476 0 0.032 0.028 0.029
| + | |
| - | 477 0 0.032 0.029 0.029
| + | |
| - | 478 0 0.032 0.029 0.029
| + | |
| - | 479 0 0.032 0.029 0.029
| + | |
| - | 480 0 0.032 0.029 0.028
| + | |
| - | 481 0 0.032 0.029 0.029
| + | |
| - | 482 0 0.033 0.029 0.029
| + | |
| - | 483 0.001 0.033 0.029 0.029
| + | |
| - | 484 0.001 0.033 0.03 0.03
| + | |
| - | 485 0 0.033 0.03 0.03
| + | |
| - | 486 0.001 0.034 0.03 0.03
| + | |
| - | 487 0.001 0.035 0.03 0.03
| + | |
| - | 488 0 0.035 0.031 0.03
| + | |
| - | 489 0.001 0.035 0.031 0.03
| + | |
| - | 490 0 0.035 0.031 0.03
| + | |
| - | 491 0 0.035 0.031 0.03
| + | |
| - | 492 0.001 0.036 0.031 0.031
| + | |
| - | 493 0 0.036 0.032 0.031
| + | |
| - | 494 0 0.037 0.032 0.031
| + | |
| - | 495 0 0.038 0.033 0.031
| + | |
| - | 496 0.001 0.038 0.033 0.031
| + | |
| - | 497 0.001 0.039 0.033 0.031
| + | |
| - | 498 0.001 0.04 0.034 0.031
| + | |
| - | 499 0.001 0.039 0.034 0.032
| + | |
| - | 500 0.001 0.04 0.034 0.032
| + | |
| - | 501 0.001 0.04 0.033 0.031
| + | |
| - | 502 0.001 0.041 0.034 0.031
| + | |
| - | 503 0 0.041 0.034 0.031
| + | |
| - | 504 0 0.04 0.034 0.031
| + | |
| - | 505 0 0.04 0.033 0.03
| + | |
| - | 506 0 0.04 0.033 0.03
| + | |
| - | 507 0 0.04 0.033 0.03
| + | |
| - | 508 0 0.04 0.033 0.03
| + | |
| - | 509 0 0.039 0.033 0.03
| + | |
| - | 510 0 0.039 0.032 0.03
| + | |
| - | 511 0 0.039 0.032 0.03
| + | |
| - | 512 0 0.038 0.032 0.03
| + | |
| - | 513 0 0.037 0.032 0.03
| + | |
| - | 514 0 0.037 0.031 0.03
| + | |
| - | 515 0 0.036 0.031 0.029
| + | |
| - | 516 0 0.036 0.031 0.03
| + | |
| - | 517 0 0.035 0.031 0.029
| + | |
| - | 518 0.001 0.035 0.031 0.03
| + | |
| - | 519 0 0.034 0.03 0.03
| + | |
| - | 520 0 0.034 0.03 0.029
| + | |
| - | 521 0 0.033 0.03 0.029
| + | |
| - | 522 0 0.033 0.029 0.029
| + | |
| - | 523 0 0.033 0.03 0.029
| + | |
| - | 524 0 0.033 0.03 0.029
| + | |
| - | 525 0 0.033 0.03 0.029
| + | |
| - | 526 0 0.033 0.03 0.029
| + | |
| - | 527 0.001 0.033 0.03 0.029
| + | |
| - | 528 0 0.034 0.03 0.029
| + | |
| - | 529 0.001 0.035 0.03 0.03
| + | |
| - | 530 0 0.035 0.031 0.03
| + | |
| - | 531 0 0.035 0.031 0.03
| + | |
| - | 532 0 0.036 0.031 0.03
| + | |
| - | 533 0 0.037 0.031 0.03
| + | |
| - | 534 0 0.038 0.032 0.031
| + | |
| - | 535 0 0.038 0.032 0.031
| + | |
| - | 536 0.001 0.039 0.033 0.031
| + | |
| - | 537 0 0.038 0.033 0.03
| + | |
| - | 538 0 0.039 0.033 0.031
| + | |
| - | 539 0 0.039 0.033 0.031
| + | |
| - | 540 0 0.04 0.033 0.031
| + | |
| - | 541 0 0.039 0.033 0.03
| + | |
| - | 542 0 0.038 0.033 0.03
| + | |
| - | 543 0 0.038 0.032 0.03
| + | |
| - | 544 0 0.039 0.033 0.031
| + | |
| - | 545 0 0.038 0.032 0.031
| + | |
| - | 546 0.001 0.037 0.032 0.03
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| - | | + | |
| - | | + | |
| - | | + | |
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| | + | [[Image:Fluorescence of NiPPIX Graph.JPG]] |
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