|
|
Line 16: |
Line 16: |
| *Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence. | | *Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence. |
|
| |
|
| Table 1: UV-VIS Results
| | [Image:Absorbance of UV-Vis Graph.JPG] |
| | |
| *Wavelength nm. Absorbance (DMF) 4um 2um 0.5um
| |
| *200 0.002 4.323 4.798 4.798
| |
| *201 0.002 4.798 4.798 4.798
| |
| *202 0.003 4.798 4.798 4.323
| |
| *203 0.002 4.798 4.798 4.798
| |
| *204 0.001 4.798 5 4.798
| |
| *205 0.002 4.798 4.798 4.798
| |
| *206 0.001 5 4.798 4.798
| |
| *207 0.001 5 5 5
| |
| *208 0.001 4.798 4.798 4.798
| |
| *209 0 5 5 5
| |
| *210 0.001 5 5 5
| |
| *211 0 5 5 5
| |
| *212 0 5 5 5
| |
| *213 -0.001 5 5 5
| |
| *214 -0.001 5 5 5
| |
| *215 -0.001 5 5 5
| |
| *216 -0.001 5 5 5
| |
| *217 -0.001 5 5 5
| |
| *218 -0.001 5 5 5
| |
| *219 0 5 5 5
| |
| *220 -0.001 5 5 5
| |
| *221 -0.001 5 5 5
| |
| *222 -0.001 5 5 5
| |
| *223 -0.001 5 5 5
| |
| *224 -0.001 5 5 5
| |
| *225 -0.001 5 5 5
| |
| *226 -0.001 5 5 5
| |
| *227 -0.001 5 5 5
| |
| *228 -0.001 5 5 5
| |
| *229 -0.001 5 5 5
| |
| *230 -0.001 5 5 5
| |
| *231 -0.001 5 5 5
| |
| *232 -0.001 5 5 5
| |
| *233 -0.001 5 5 5
| |
| *234 -0.001 5 5 5
| |
| *235 -0.001 5 5 5
| |
| *236 -0.001 5 5 5
| |
| *237 -0.001 5 5 5
| |
| *238 -0.001 5 5 5
| |
| *239 -0.001 5 5 5
| |
| *240 -0.001 5 5 5
| |
| *241 -0.001 5 5 5
| |
| *242 -0.001 5 5 5
| |
| *243 -0.001 5 5 5
| |
| *244 -0.001 5 5 5
| |
| *245 -0.001 5 5 5
| |
| *246 -0.001 5 5 5
| |
| *247 -0.001 5 5 5
| |
| *248 -0.001 5 5 5
| |
| *249 -0.001 5 5 5
| |
| *250 -0.001 5 5 4.798
| |
| *251 -0.001 5 5 4.798
| |
| *252 -0.001 5 5 5
| |
| *253 -0.001 5 5 5
| |
| *254 -0.001 5 5 5
| |
| *255 -0.001 5 5 5
| |
| *256 -0.001 5 5 5
| |
| *257 -0.001 5 5 4.798
| |
| *258 -0.001 5 5 5
| |
| *259 -0.001 4.798 5 5
| |
| *260 -0.001 4.798 4.798 4.798
| |
| *261 -0.001 4.798 4.798 5
| |
| *262 -0.001 3.848 4.323 4.323
| |
| *263 -0.001 2.979 3.525 3.688
| |
| *264 -0.001 2.24 2.699 2.819
| |
| *265 0 1.659 2.002 2.095
| |
| *266 -0.001 1.246 1.494 1.569
| |
| *267 -0.001 0.937 1.121 1.17
| |
| *268 -0.001 0.715 0.844 0.878
| |
| *269 -0.001 0.567 0.66 0.687
| |
| *270 -0.001 0.463 0.534 0.555
| |
| *271 -0.001 0.391 0.443 0.457
| |
| *272 0 0.34 0.378 0.388
| |
| *273 0 0.304 0.332 0.34
| |
| *274 0 0.278 0.302 0.307
| |
| *275 -0.001 0.259 0.279 0.283
| |
| *276 -0.001 0.243 0.26 0.264
| |
| *277 -0.002 0.231 0.246 0.249
| |
| *278 -0.002 0.222 0.235 0.237
| |
| *279 -0.001 0.213 0.226 0.227
| |
| *280 0 0.207 0.217 0.219
| |
| *281 -0.001 0.2 0.209 0.211
| |
| *282 0 0.194 0.202 0.204
| |
| *283 0 0.188 0.195 0.197
| |
| *284 -0.001 0.183 0.189 0.19
| |
| *285 -0.001 0.177 0.183 0.184
| |
| *286 -0.001 0.173 0.178 0.179
| |
| *287 -0.001 0.167 0.173 0.173
| |
| *288 0 0.163 0.167 0.167
| |
| *289 -0.001 0.158 0.161 0.162
| |
| *290 -0.001 0.152 0.155 0.156
| |
| *291 -0.002 0.147 0.15 0.15
| |
| *292 -0.001 0.142 0.145 0.144
| |
| *293 -0.001 0.138 0.139 0.139
| |
| *294 -0.001 0.133 0.134 0.134
| |
| *295 -0.001 0.129 0.13 0.13
| |
| *296 -0.001 0.125 0.126 0.126
| |
| *297 -0.001 0.122 0.121 0.121
| |
| *298 -0.001 0.118 0.117 0.117
| |
| *299 -0.001 0.113 0.113 0.113
| |
| *300 -0.001 0.111 0.109 0.109
| |
| *301 -0.001 0.107 0.106 0.106
| |
| *302 0 0.106 0.102 0.103
| |
| *303 0 0.103 0.1 0.1
| |
| *304 -0.001 0.1 0.097 0.096
| |
| *305 -0.001 0.097 0.093 0.093
| |
| *306 -0.001 0.094 0.091 0.091
| |
| *307 -0.001 0.091 0.089 0.087
| |
| *308 -0.001 0.089 0.086 0.085
| |
| *309 0 0.087 0.083 0.082
| |
| *310 -0.001 0.085 0.08 0.079
| |
| *311 0 0.083 0.079 0.077
| |
| *312 -0.001 0.081 0.076 0.076
| |
| *313 0 0.08 0.075 0.073
| |
| *314 0 0.079 0.073 0.072
| |
| *315 -0.001 0.077 0.071 0.07
| |
| *316 -0.001 0.076 0.07 0.068
| |
| *317 0 0.075 0.068 0.067
| |
| *318 -0.001 0.074 0.068 0.066
| |
| *319 -0.001 0.073 0.066 0.064
| |
| *320 -0.001 0.072 0.065 0.063
| |
| *321 -0.001 0.071 0.064 0.063
| |
| *322 -0.001 0.07 0.062 0.061
| |
| *323 -0.001 0.07 0.062 0.06
| |
| *324 -0.001 0.069 0.061 0.059
| |
| *325 -0.001 0.069 0.061 0.058
| |
| *326 0 0.068 0.06 0.056
| |
| *327 -0.001 0.068 0.059 0.056
| |
| *328 -0.001 0.068 0.059 0.056
| |
| *329 0 0.067 0.058 0.054
| |
| *330 -0.001 0.067 0.058 0.054
| |
| *331 -0.001 0.067 0.056 0.053
| |
| *332 -0.001 0.067 0.057 0.052
| |
| *333 -0.001 0.067 0.057 0.053
| |
| *334 -0.001 0.066 0.055 0.052
| |
| *335 -0.001 0.066 0.055 0.051
| |
| *336 -0.001 0.066 0.056 0.052
| |
| *337 -0.001 0.067 0.055 0.05
| |
| *338 -0.001 0.067 0.054 0.05
| |
| *339 -0.001 0.067 0.055 0.049
| |
| *340 -0.002 0.065 0.053 0.048
| |
| *341 -0.001 0.067 0.054 0.048
| |
| *342 -0.001 0.066 0.053 0.048
| |
| *343 0 0.067 0.054 0.049
| |
| *344 0 0.067 0.053 0.048
| |
| *345 -0.001 0.067 0.054 0.047
| |
| *346 -0.001 0.067 0.053 0.047
| |
| *347 0 0.067 0.054 0.046
| |
| *348 -0.001 0.067 0.053 0.046
| |
| *349 -0.001 0.067 0.052 0.046
| |
| *350 -0.001 0.069 0.053 0.046
| |
| *351 0 0.068 0.053 0.046
| |
| *352 0 0.07 0.053 0.044
| |
| *353 0 0.07 0.053 0.045
| |
| *354 -0.001 0.07 0.054 0.045
| |
| *355 -0.002 0.072 0.054 0.044
| |
| *356 0 0.073 0.054 0.044
| |
| *357 0 0.074 0.055 0.044
| |
| *358 -0.001 0.075 0.054 0.043
| |
| *359 -0.001 0.075 0.056 0.043
| |
| *360 0.001 0.077 0.057 0.046
| |
| *361 -0.001 0.076 0.055 0.042
| |
| *362 0 0.077 0.055 0.042
| |
| *363 -0.001 0.078 0.055 0.042
| |
| *364 -0.001 0.079 0.055 0.042
| |
| *365 -0.001 0.08 0.056 0.041
| |
| *366 0 0.082 0.057 0.041
| |
| *367 0 0.084 0.058 0.042
| |
| *368 0 0.086 0.059 0.042
| |
| *369 0 0.087 0.06 0.042
| |
| *370 -0.001 0.089 0.06 0.042
| |
| *371 -0.001 0.091 0.061 0.041
| |
| *372 -0.001 0.093 0.062 0.042
| |
| *373 -0.001 0.096 0.063 0.042
| |
| *374 0 0.099 0.065 0.042
| |
| *375 -0.001 0.102 0.067 0.044
| |
| *376 -0.001 0.104 0.067 0.044
| |
| *377 0 0.107 0.069 0.044
| |
| *378 0 0.11 0.071 0.044
| |
| *379 0 0.112 0.072 0.044
| |
| *380 0 0.115 0.074 0.044
| |
| *381 -0.001 0.118 0.074 0.045
| |
| *382 0 0.12 0.076 0.045
| |
| *383 0 0.123 0.077 0.045
| |
| *384 0 0.125 0.078 0.044
| |
| *385 0 0.127 0.079 0.044
| |
| *386 0 0.13 0.08 0.044
| |
| *387 0 0.132 0.082 0.044
| |
| *388 -0.001 0.135 0.082 0.044
| |
| *389 -0.001 0.137 0.084 0.044
| |
| *390 -0.001 0.141 0.086 0.044
| |
| *391 -0.001 0.145 0.087 0.045
| |
| *392 0 0.148 0.09 0.045
| |
| *393 0 0.152 0.091 0.045
| |
| *394 -0.001 0.155 0.093 0.046
| |
| *395 0 0.16 0.095 0.046
| |
| *396 0 0.164 0.097 0.047
| |
| *397 0 0.167 0.099 0.047
| |
| *398 0 0.17 0.101 0.048
| |
| *399 0.001 0.174 0.103 0.048
| |
| *400 0 0.177 0.104 0.049
| |
| *401 0 0.18 0.106 0.049
| |
| *402 0 0.182 0.107 0.049
| |
| *403 0 0.183 0.108 0.049
| |
| *404 0 0.184 0.109 0.049
| |
| *405 0 0.183 0.108 0.049
| |
| *406 0 0.184 0.108 0.049
| |
| *407 0 0.182 0.107 0.049
| |
| *408 0 0.181 0.106 0.049
| |
| *409 0 0.178 0.105 0.049
| |
| *410 0 0.173 0.103 0.048
| |
| *411 0 0.17 0.101 0.048
| |
| *412 0 0.166 0.098 0.047
| |
| *413 0 0.161 0.095 0.047
| |
| *414 0 0.155 0.093 0.047
| |
| *415 0 0.15 0.09 0.046
| |
| *416 0 0.144 0.087 0.045
| |
| *417 0.001 0.138 0.084 0.044
| |
| *418 0.001 0.132 0.08 0.044
| |
| *419 0 0.126 0.077 0.043
| |
| *420 -0.001 0.12 0.073 0.041
| |
| *421 0.001 0.112 0.069 0.041
| |
| *422 0.001 0.106 0.066 0.039
| |
| *423 0.001 0.1 0.063 0.039
| |
| *424 0 0.094 0.059 0.038
| |
| *425 0 0.087 0.057 0.037
| |
| *426 -0.001 0.081 0.054 0.036
| |
| *427 0 0.076 0.051 0.035
| |
| *428 -0.001 0.071 0.049 0.034
| |
| *429 0 0.067 0.046 0.033
| |
| *430 -0.001 0.063 0.044 0.033
| |
| *431 0 0.06 0.043 0.032
| |
| *432 0 0.057 0.042 0.032
| |
| *433 0 0.055 0.04 0.031
| |
| *434 0 0.052 0.039 0.031
| |
| *435 0 0.05 0.038 0.031
| |
| *436 -0.001 0.048 0.037 0.031
| |
| *437 0 0.046 0.036 0.03
| |
| *438 -0.001 0.045 0.035 0.03
| |
| *439 -0.001 0.043 0.034 0.029
| |
| *440 0 0.042 0.034 0.029
| |
| *441 0.001 0.041 0.033 0.03
| |
| *442 0 0.04 0.032 0.03
| |
| *443 0 0.039 0.032 0.029
| |
| *444 0 0.038 0.032 0.029
| |
| *445 0 0.037 0.031 0.029
| |
| *446 0 0.037 0.031 0.029
| |
| *447 0 0.036 0.03 0.029
| |
| *448 0 0.036 0.031 0.029
| |
| *449 -0.001 0.035 0.03 0.029
| |
| *450 0 0.034 0.03 0.028
| |
| *451 0.001 0.035 0.03 0.029
| |
| *452 0 0.035 0.03 0.03
| |
| *453 0 0.034 0.03 0.029
| |
| *454 -0.001 0.034 0.03 0.03
| |
| *455 0 0.034 0.03 0.029
| |
| *456 0 0.034 0.03 0.029
| |
| *457 0 0.033 0.029 0.029
| |
| *458 0 0.032 0.029 0.029
| |
| *459 0.001 0.033 0.029 0.03
| |
| *460 0 0.033 0.03 0.03
| |
| *461 0 0.032 0.029 0.029
| |
| *462 0 0.032 0.029 0.029
| |
| *463 0 0.032 0.029 0.029
| |
| *464 0 0.032 0.029 0.029
| |
| *465 0 0.032 0.028 0.028
| |
| *466 0 0.032 0.028 0.028
| |
| *467 0 0.031 0.028 0.028
| |
| *468 0 0.031 0.028 0.028
| |
| *469 0 0.031 0.028 0.028
| |
| *470 0 0.031 0.028 0.028
| |
| *471 0 0.031 0.028 0.028
| |
| *472 0.001 0.032 0.028 0.029
| |
| *473 0 0.031 0.028 0.028
| |
| *474 0 0.031 0.028 0.028
| |
| *475 0 0.032 0.028 0.028
| |
| *476 0 0.032 0.028 0.029
| |
| *477 0 0.032 0.029 0.029
| |
| *478 0 0.032 0.029 0.029
| |
| *479 0 0.032 0.029 0.029
| |
| *480 0 0.032 0.029 0.028
| |
| *481 0 0.032 0.029 0.029
| |
| *482 0 0.033 0.029 0.029
| |
| *483 0.001 0.033 0.029 0.029
| |
| *484 0.001 0.033 0.03 0.03
| |
| *485 0 0.033 0.03 0.03
| |
| *486 0.001 0.034 0.03 0.03
| |
| *487 0.001 0.035 0.03 0.03
| |
| *488 0 0.035 0.031 0.03
| |
| *489 0.001 0.035 0.031 0.03
| |
| *490 0 0.035 0.031 0.03
| |
| *491 0 0.035 0.031 0.03
| |
| *492 0.001 0.036 0.031 0.031
| |
| *493 0 0.036 0.032 0.031
| |
| *494 0 0.037 0.032 0.031
| |
| *495 0 0.038 0.033 0.031
| |
| *496 0.001 0.038 0.033 0.031
| |
| *497 0.001 0.039 0.033 0.031
| |
| *498 0.001 0.04 0.034 0.031
| |
| *499 0.001 0.039 0.034 0.032
| |
| *500 0.001 0.04 0.034 0.032
| |
| *501 0.001 0.04 0.033 0.031
| |
| *502 0.001 0.041 0.034 0.031
| |
| *503 0 0.041 0.034 0.031
| |
| *504 0 0.04 0.034 0.031
| |
| *505 0 0.04 0.033 0.03
| |
| *506 0 0.04 0.033 0.03
| |
| *507 0 0.04 0.033 0.03
| |
| *508 0 0.04 0.033 0.03
| |
| *509 0 0.039 0.033 0.03
| |
| *510 0 0.039 0.032 0.03
| |
| *511 0 0.039 0.032 0.03
| |
| *512 0 0.038 0.032 0.03
| |
| *513 0 0.037 0.032 0.03
| |
| *514 0 0.037 0.031 0.03
| |
| *515 0 0.036 0.031 0.029
| |
| *516 0 0.036 0.031 0.03
| |
| *517 0 0.035 0.031 0.029
| |
| *518 0.001 0.035 0.031 0.03
| |
| *519 0 0.034 0.03 0.03
| |
| *520 0 0.034 0.03 0.029
| |
| *521 0 0.033 0.03 0.029
| |
| *522 0 0.033 0.029 0.029
| |
| *523 0 0.033 0.03 0.029
| |
| *524 0 0.033 0.03 0.029
| |
| *525 0 0.033 0.03 0.029
| |
| *526 0 0.033 0.03 0.029
| |
| *527 0.001 0.033 0.03 0.029
| |
| *528 0 0.034 0.03 0.029
| |
| *529 0.001 0.035 0.03 0.03
| |
| *530 0 0.035 0.031 0.03
| |
| *531 0 0.035 0.031 0.03
| |
| *532 0 0.036 0.031 0.03
| |
| *533 0 0.037 0.031 0.03
| |
| *534 0 0.038 0.032 0.031
| |
| *535 0 0.038 0.032 0.031
| |
| *536 0.001 0.039 0.033 0.031
| |
| *537 0 0.038 0.033 0.03
| |
| *538 0 0.039 0.033 0.031
| |
| *539 0 0.039 0.033 0.031
| |
| *540 0 0.04 0.033 0.031
| |
| *541 0 0.039 0.033 0.03
| |
| *542 0 0.038 0.033 0.03
| |
| *543 0 0.038 0.032 0.03
| |
| *544 0 0.039 0.033 0.031
| |
| *545 0 0.038 0.032 0.031
| |
| *546 0.001 0.037 0.032 0.03
| |
| *547 0 0.036 0.032 0.031
| |
| *548 0 0.036 0.031 0.03
| |
| *549 0 0.035 0.031 0.03
| |
| *550 0 0.035 0.03 0.03
| |
| *551 0 0.034 0.03 0.03
| |
| *552 0 0.035 0.03 0.03
| |
| *553 0 0.034 0.03 0.03
| |
| *554 0 0.034 0.03 0.03
| |
| *555 0 0.034 0.03 0.03
| |
| *556 0 0.034 0.03 0.03
| |
| *557 0 0.034 0.03 0.029
| |
| *558 0 0.034 0.03 0.029
| |
| *559 0 0.034 0.03 0.03
| |
| *560 0 0.034 0.03 0.029
| |
| *561 0 0.034 0.03 0.03
| |
| *562 0 0.034 0.03 0.03
| |
| *563 0 0.034 0.03 0.03
| |
| *564 0 0.034 0.03 0.029
| |
| *565 0 0.034 0.03 0.03
| |
| *566 0.001 0.034 0.03 0.03
| |
| *567 0.001 0.034 0.03 0.03
| |
| *568 0 0.034 0.03 0.03
| |
| *569 0 0.034 0.03 0.03
| |
| *570 0 0.034 0.03 0.03
| |
| *571 0 0.034 0.03 0.03
| |
| *572 0 0.035 0.03 0.03
| |
| *573 0 0.035 0.031 0.03
| |
| *574 0 0.035 0.031 0.03
| |
| *575 0 0.035 0.031 0.03
| |
| *576 0 0.034 0.03 0.03
| |
| *577 0 0.035 0.03 0.03
| |
| *578 0 0.034 0.03 0.03
| |
| *579 0 0.034 0.03 0.03
| |
| *580 0 0.034 0.03 0.03
| |
| *581 0 0.034 0.03 0.03
| |
| *582 0 0.034 0.03 0.03
| |
| *583 0 0.033 0.03 0.03
| |
| *584 0 0.034 0.03 0.03
| |
| *585 0 0.033 0.03 0.03
| |
| *586 0 0.033 0.029 0.03
| |
| *587 0 0.033 0.03 0.03
| |
| *588 0.001 0.032 0.03 0.03
| |
| *589 0.001 0.032 0.029 0.03
| |
| *590 0 0.032 0.029 0.03
| |
| *591 0 0.031 0.029 0.03
| |
| *592 0 0.031 0.029 0.029
| |
| *593 0 0.031 0.028 0.029
| |
| *594 0 0.03 0.029 0.029
| |
| *595 0 0.03 0.028 0.03
| |
| *596 0 0.03 0.028 0.029
| |
| *597 0 0.03 0.028 0.03
| |
| *598 0 0.03 0.028 0.03
| |
| *599 0 0.03 0.028 0.029
| |
| *600 0 0.029 0.028 0.029
| |
| *601 0 0.03 0.028 0.029
| |
| *602 0.001 0.029 0.028 0.029
| |
| *603 0 0.03 0.028 0.029
| |
| *604 0 0.03 0.028 0.029
| |
| *605 0 0.029 0.028 0.029
| |
| *606 0 0.029 0.028 0.029
| |
| *607 0 0.029 0.028 0.029
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