User:Paul Rothenberg/Notebook/Pauls Notebook/2014/02/19: Difference between revisions
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==Synthesis of Manganese PPIX== | ==Synthesis of Manganese PPIX== | ||
* Today, Dhea and I are going to synthesize MnPPIX in DMF under the presence of nitrogen. We are going to follow the Adler protocol for the synthesis, as I did back in 2012 | * Today, Dhea and I are going to synthesize MnPPIX in DMF under the presence of nitrogen. We are going to follow the Adler protocol for the synthesis, as I did [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2012/09/19#19_September_2012| back in 2012]. | ||
*Procedure: | *Procedure: | ||
# 50 mL of DMF was brought to reflux in a 19/22 round bottom flask with a 100 V Volt-ac heating pad with a stir bar under the presence of N<sub>2</sub> gas | # 50 mL of DMF was brought to reflux in a 19/22 round bottom flask with a 100 V Volt-ac heating pad with a stir bar under the presence of N<sub>2</sub> gas | ||
# 499.3 mg of PPIX was measured out and added to the DMF once the DMF began to reflux | # 499.3 mg of PPIX was measured out and added to the DMF once the DMF began to reflux | ||
# 364.1 mg of Manganese Acetate was measured out and dissolved in a minimum | # 364.1 mg of Manganese Acetate was measured out and dissolved in a minimum volume of DMF | ||
# The Manganese dissolved in DMF was added to the refluxing solution using a needle and a syringe | # The Manganese dissolved in DMF was added to the refluxing solution using a needle and a syringe | ||
# The solution was let reflux for 30 minutes | # The solution was let reflux for 30 minutes | ||
# The solution was then removed from the heating pad and placed in an ice bath for 15 minutes | |||
# 500 mL of chilled water was then added and let chill for 10 minutes | |||
# The solution was then filtered with a vacuum setup and rinsed with water | |||
# The filter paper was determined to be 0.1058 grams before filtration. | |||
Revision as of 11:36, 19 February 2014
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Synthesis of Manganese PPIX
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