User:Rebeca Rodriguez/Notebook/581/2014/08/27: Difference between revisions
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==Description== | ==Description== | ||
Perform the following procedures (1 and 2) in parallel for the start to the synthesis of cross-linked polymer and cross-linked polymer-clay films. | |||
Description of todays protocol taken from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/08/27|08-27-14]] | |||
link to prepared the starting materials from [[User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/26|Matt Hartings Notebook]] | |||
# Polymer-Clay Films | |||
## Add 7mL of water to 1.0023g of 22,000MW polyvinyl alcohol and 0.1102g of sodium montmorillonite in a glass vial | |||
## Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes) | |||
## Cool the solution to room temperature | |||
## Add 0.5mL 0.8 wt% glutaraldehyde. | |||
### NOTE: Perform step 4 in the hood | |||
## Stir for an additional 3 minutes to ensure homogeneity | |||
## Pour solution into a teflon dish to dry until the next class | |||
# Polymer Films | |||
## Add 7mL of water to 1.006g of 22,000MW polyvinyl alcohol in a glass vial | |||
## Stir the solution with constant heating at 75C until the polymer is dissolved (~15 minutes) | |||
## Cool the solution to room temperature | |||
## Add 0.5mL 0.8 wt% glutaraldehyde. | |||
### NOTE: Perform step 4 in the hood | |||
## Stir for an additional 3 minutes to ensure homogeneity | |||
## Pour solution into a teflon dish to dry until the next class |
Latest revision as of 10:37, 30 August 2014
Description
Perform the following procedures (1 and 2) in parallel for the start to the synthesis of cross-linked polymer and cross-linked polymer-clay films.
Description of todays protocol taken from 08-27-14 link to prepared the starting materials from Matt Hartings Notebook
- Polymer-Clay Films
- Add 7mL of water to 1.0023g of 22,000MW polyvinyl alcohol and 0.1102g of sodium montmorillonite in a glass vial
- Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes)
- Cool the solution to room temperature
- Add 0.5mL 0.8 wt% glutaraldehyde.
- NOTE: Perform step 4 in the hood
- Stir for an additional 3 minutes to ensure homogeneity
- Pour solution into a teflon dish to dry until the next class
- Polymer Films
- Add 7mL of water to 1.006g of 22,000MW polyvinyl alcohol in a glass vial
- Stir the solution with constant heating at 75C until the polymer is dissolved (~15 minutes)
- Cool the solution to room temperature
- Add 0.5mL 0.8 wt% glutaraldehyde.
- NOTE: Perform step 4 in the hood
- Stir for an additional 3 minutes to ensure homogeneity
- Pour solution into a teflon dish to dry until the next class