User:Rebeca Rodriguez/Notebook/581/2014/09/24: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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==Objective==
==Objective==
Learn how to maintain an OpenWetWare Notebook.
# Continue processing films from last week
# Make two new films
## One containing the exchanged clay that your group made
###0.9995g of PVA with 0.1107g of 1-hexadecyltriphenylphosphonium bromide
## One containing the exchanged clay that another group made
###1.0022g of PVA with 0.1111g of tributylhexadecylphosphonium bromide used from [[User:Michael_S._Bible/Notebook/581|Michael's]] group
# Run AA on the arsenic samples
## Make As standards (Note: AA will consume around 5mL of sample)
### 0ppm
### 10ppm
### 20ppm
### 30ppm
### 40ppm
### 50 ppm
## Dilute your samples so that their original concentration falls somewhere in this range.
## Make calibration curve and determine the concentration of As using AA.


==Description==
==Description==
Line 17: Line 32:


==Data==
==Data==
* Add data and results here...


==Notes==
===R6G soaked in PVA Film===
This area is for any observations or conclusions that you would like to note.


{| {{table}}
| align="center" style="background:#f0f0f0;"|'''PVA'''
| align="center" style="background:#f0f0f0;"|'''Concentration (micromL)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Vial (g)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Vial and Film (g)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Film (g)'''
|-
| 1||1||16.4096||16.5057||0.0961
|-
| 2||10||16.5198||16.6298||0.11
|-
| 3||20||16.3885||16.5115||0.123
|-
|
|}


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
===R6G soaked in PVAC Film===
 
[[Category:Course]]
[[Category:Miscellaneous]]
 
 
 
[[Category:Course]]
[[Category:Miscellaneous]]


{| {{table}}
| align="center" style="background:#f0f0f0;"|'''PVAC'''
| align="center" style="background:#f0f0f0;"|'''Concentration (micromL)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Vial (g)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Vial and Film (g)'''
| align="center" style="background:#f0f0f0;"|'''Mass of Film (g)'''
|-
| 4||1||16.3905||16.4411||0.0506
|-
| 5||10||16.3518||16.4301||0.0783
|-
| 6||20||16.3959||16.4812||0.0853
|-
|
|}


====Preparation of solutions====
* Stock solution was 159uM
#1uM R6G - 0.629 mL of stock into 100mL
#10uM R6G - 6.289 mL of stock into 100mL
#20uM R6G - 12.578mL of stock into 100mL




Latest revision as of 00:21, 27 September 2017

Biomaterials Design Lab Main project page
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Objective

  1. Continue processing films from last week
  2. Make two new films
    1. One containing the exchanged clay that your group made
      1. 0.9995g of PVA with 0.1107g of 1-hexadecyltriphenylphosphonium bromide
    2. One containing the exchanged clay that another group made
      1. 1.0022g of PVA with 0.1111g of tributylhexadecylphosphonium bromide used from Michael's group
  3. Run AA on the arsenic samples
    1. Make As standards (Note: AA will consume around 5mL of sample)
      1. 0ppm
      2. 10ppm
      3. 20ppm
      4. 30ppm
      5. 40ppm
      6. 50 ppm
    2. Dilute your samples so that their original concentration falls somewhere in this range.
    3. Make calibration curve and determine the concentration of As using AA.

Description

  1. Add experimental record here. Include what, how, and why...

Data

R6G soaked in PVA Film

PVA Concentration (micromL) Mass of Vial (g) Mass of Vial and Film (g) Mass of Film (g)
1 1 16.4096 16.5057 0.0961
2 10 16.5198 16.6298 0.11
3 20 16.3885 16.5115 0.123

R6G soaked in PVAC Film

PVAC Concentration (micromL) Mass of Vial (g) Mass of Vial and Film (g) Mass of Film (g)
4 1 16.3905 16.4411 0.0506
5 10 16.3518 16.4301 0.0783
6 20 16.3959 16.4812 0.0853

Preparation of solutions

  • Stock solution was 159uM
  1. 1uM R6G - 0.629 mL of stock into 100mL
  2. 10uM R6G - 6.289 mL of stock into 100mL
  3. 20uM R6G - 12.578mL of stock into 100mL



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