User:Rebeca Rodriguez/Notebook/Chem 471/2015/09/22: Difference between revisions
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|style="background-color: #EEE"|[[Image: | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | |style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | ||
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<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### --> | <!-- ##### DO NOT edit above this line unless you know what you are doing. ##### --> | ||
==Objective== | ==Objective== | ||
# Run DSC on gold nano fibers | |||
# Run PXRD on gold nano fibers + playdoh | |||
# Run FTIR on gold nano fibers | |||
==Protocol== | |||
Samples of AuNP Fibers were obtained by centrifuging several 5 mL samples of fiber containing solutions at 4000 RPM for 5 minutes in 15 ml Falcon tubes and then pipetting off the supernatant fluid. | |||
Each DSC sample was setup to run through 3 temperature cycles with a ramp speed of 5 °C/min | |||
* 1 sample of Lysozyme was ramped from 20 °C to 100 °C | |||
* 1 sample of Lysozyme was ramped from 20 °C to 200 °C | |||
* 1 sample of AuNP fibers was ramped from 20 °C to 100 °C | |||
* 1 sample of AuNP fibers was ramped from 20 °C to 200 °C | |||
==Results== | |||
[[Image:FTIR_of_Lysozyme.png|1000px]] | |||
FTIR Spectrum of Lysozyme. | |||
[[ | [[Image:FTIR_of_AuNP_Fibers.png|1000px]] | ||
FTIR Spectrum of the AuNP Fibers. | |||
Revision as of 19:34, 7 October 2015
Project name | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
Objective
ProtocolSamples of AuNP Fibers were obtained by centrifuging several 5 mL samples of fiber containing solutions at 4000 RPM for 5 minutes in 15 ml Falcon tubes and then pipetting off the supernatant fluid. Each DSC sample was setup to run through 3 temperature cycles with a ramp speed of 5 °C/min
ResultsFTIR Spectrum of Lysozyme. FTIR Spectrum of the AuNP Fibers.
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