User:Samiye Yaman/Notebook/Lab 581/2012/11/02: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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*At 70C place the film into beaker.
*At 70C place the film into beaker.


==Data==


'''48 hours After placing porphyrin film into 1 % HCl solution'''
'''Part 2'''


*The film became full green.(compared to the pictures on 31/10/2012)
*FTIR measurement for every film that has been prepared.


[[Image:2012-11-02_12.14.36.jpg|500px]]
==Data==


'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''


*Before cross-linking
'''*Before cross-linking'''


*The film shrunk and look more brittle.
*The film shrunk and look more brittle.
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[[Image:2012-10-31_11.23.11.jpg|500px]]
[[Image:2012-10-31_11.23.11.jpg|500px]]
'''*After cross-linking'''
*The film expanded a little.
*Less intense green color and looked more reddish brown.
[[Image:2012-11-07_08.38.59.jpg|500px]]
'''FTIR Results'''
[[Image:1g22000PVOHcrosslinked.png|500px]]
[[Image:1g22000PVOHH3PO4MaleicAcid.png|500px]]
[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png|500px]]
[[Image:1gPVOH22000H3PO4.png|500px]]
[[Image:1gPVOH100000.png|500px]]
[[Image:1gPVOH100000HCl.png|500px]]
[[Image:1gPVOH100000HClcrosslinked.png|500px]]
[[Image:Halfg22000PVOHgluteraldehyde.png|500px]]
[[Image:Halfg100000PVOHcrosslinked.png|500px]]
[[Image:HalfgPVOH2200.png|500px]]
[[Image:HalfgPVOH22000H3PO4.png|500px]]
[[Image:HalfgPVOH100000HCl.png|500px]]
[[Image:HalfgPVOH100000HClSuccinicAcid.png|500px]]
[[Image:OnetenthgPVOH22000.png|500px]]
[[Image:OnetenthgPVOH100000.png|500px]]


==Notes==
==Notes==

Latest revision as of 22:11, 26 September 2017

Experimental Chemistry Main project page
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Objective

Description

Part 1

  • Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.
  • Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.
  • At 70C place the film into beaker.


Part 2

  • FTIR measurement for every film that has been prepared.

Data

Porphyrin film with 2 drops of HCL, prepared on 24/10/2012

*Before cross-linking

  • The film shrunk and look more brittle.
  • More intense green color.

*After cross-linking

  • The film expanded a little.
  • Less intense green color and looked more reddish brown.


FTIR Results


Notes

This area is for any observations or conclusions that you would like to note.


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.



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