User:Samiye Yaman/Notebook/Lab 581/2012/11/07 - Revision history

Samiye Yaman: /* Data */

2012-11-07T16:36:02Z

Data

←Older revision		Revision as of 16:36, 7 November 2012
Line 36:		Line 36:

	==Data==		==Data==
		+
		+	*Film 1 dissolved during the filtration.

	'''DSE Results'''		'''DSE Results'''

Samiye Yaman: /* Data */

2012-11-07T16:35:14Z

Data

←Older revision		Revision as of 16:35, 7 November 2012
Line 37:		Line 37:
	==Data==		==Data==

-	'''~~Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''~~	+	'''DSE Results'''
-		+
-	*Before cross-linking	+
-		+
-	*The film shrunk and look more brittle.	+
-		+
-	*More intense green color.	+
-		+
-	~~[[Image:2012-10-31_11.23.11.jpg\|500px]]~~	+
-		+
-		+
-	~~'''FTIR~~ Results'''	+
-		+
-	~~[[Image:1g22000PVOHcrosslinked.png\|500px]]~~	+
-		+
-		+
-	~~[[Image:1g22000PVOHH3PO4MaleicAcid.png\|500px]]~~	+
-		+
-	~~[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH22000H3PO4.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000HCl.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000HClcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:Halfg22000PVOHgluteraldehyde.png\|500px]]~~	+
-		+
-	~~[[Image:Halfg100000PVOHcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH2200.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH22000H3PO4.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH100000HCl.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH100000HClSuccinicAcid.png\|500px]]~~	+
-		+
-	~~[[Image:OnetenthgPVOH22000.png\|500px]]~~	+
-		+
-	~~[[Image:OnetenthgPVOH100000.png\|500px]]~~	+

	==Notes==		==Notes==

Samiye Yaman: /* Description */

2012-11-07T16:33:58Z

Description

←Older revision		Revision as of 16:33, 7 November 2012
Line 29:		Line 29:
	1) 0.5g PVOH, gluteraldehyde (1ml)		1) 0.5g PVOH, gluteraldehyde (1ml)

-	2)0.5 g PVOH (100000)+HCl+ Succinate acid	+	2) 0.5 g PVOH (100000)+HCl+ Succinate acid

-	3)0.5 g PVOH (22000)+ 3 ml water + Mallic acid + phosphoric acid	+	3) 0.5 g PVOH (22000)+ 3 ml water + Mallic acid + phosphoric acid

	4) 1 g PVOH (22000) + phosphoric acid + Mallic acid		4) 1 g PVOH (22000) + phosphoric acid + Mallic acid

Samiye Yaman: /* Description */

2012-11-07T16:32:04Z

Description

←Older revision		Revision as of 16:32, 7 November 2012
Line 12:		Line 12:
	==Description==		==Description==

-	'''Part 1 '''	+	'''Part 1: Filtration with different kinds of film'''

-	*~~Place the porphyrin film~~ (~~with 2 drops of HCL~~)~~, prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.~~	+	*Film 1: 0.5g PVOH, gluteraldehyde (1ml)

-	*~~Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.~~	+	*Film 2: NaMT PVOH

-	*~~At 70C place the film into beaker~~.	+	*Use 20 ml of CuSO4 during each filtration.
		+
		+	*Filtration done with 3 different timings. 10 minutes, 30 minutes and 1 hour.


	'''Part 2'''		'''Part 2'''

-	*~~FTIR~~ measurement for ~~every film that has been prepared~~.	+	*DSE measurement for
		+
		+	1) 0.5g PVOH, gluteraldehyde (1ml)
		+
		+	2)0.5 g PVOH (100000)+HCl+ Succinate acid
		+
		+	3)0.5 g PVOH (22000)+ 3 ml water + Mallic acid + phosphoric acid
		+
		+	4) 1 g PVOH (22000) + phosphoric acid + Mallic acid

	==Data==		==Data==

Samiye Yaman at 16:18, 7 November 2012

2012-11-07T16:18:05Z

←Older revision		Revision as of 16:18, 7 November 2012
Line 8:		Line 8:


		+	==Objective==

		+	==Description==
		+
		+	'''Part 1 '''
		+
		+	*Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.
		+
		+	*Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.
		+
		+	*At 70C place the film into beaker.
		+
		+
		+	'''Part 2'''
		+
		+	*FTIR measurement for every film that has been prepared.
		+
		+	==Data==
		+
		+	'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
		+
		+	*Before cross-linking
		+
		+	*The film shrunk and look more brittle.
		+
		+	*More intense green color.
		+
		+	[[Image:2012-10-31_11.23.11.jpg\|500px]]
		+
		+
		+	'''FTIR Results'''
		+
		+	[[Image:1g22000PVOHcrosslinked.png\|500px]]
		+
		+
		+	[[Image:1g22000PVOHH3PO4MaleicAcid.png\|500px]]
		+
		+	[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png\|500px]]
		+
		+	[[Image:1gPVOH22000H3PO4.png\|500px]]
		+
		+	[[Image:1gPVOH100000.png\|500px]]
		+
		+	[[Image:1gPVOH100000HCl.png\|500px]]
		+
		+	[[Image:1gPVOH100000HClcrosslinked.png\|500px]]
		+
		+	[[Image:Halfg22000PVOHgluteraldehyde.png\|500px]]
		+
		+	[[Image:Halfg100000PVOHcrosslinked.png\|500px]]
		+
		+	[[Image:HalfgPVOH2200.png\|500px]]
		+
		+	[[Image:HalfgPVOH22000H3PO4.png\|500px]]
		+
		+	[[Image:HalfgPVOH100000HCl.png\|500px]]
		+
		+	[[Image:HalfgPVOH100000HClSuccinicAcid.png\|500px]]
		+
		+	[[Image:OnetenthgPVOH22000.png\|500px]]
		+
		+	[[Image:OnetenthgPVOH100000.png\|500px]]
		+
		+	==Notes==
		+	This area is for any observations or conclusions that you would like to note.
		+
		+
		+	Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
		+
		+	[[Category:Course]]
		+	[[Category:Miscellaneous]]


-	~~==Description==~~
-
-	*The course is designed by American University to experiment different aspects of PVOH films.

-	*During the course PVOH films with different molecular weight will be produced. Effects of cross-~~linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested~~.	+	<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
		+	\|}

-	*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.	+	__NOTOC__

Samiye Yaman: Autocreate 2012/11/07 Entry for User:Samiye_Yaman/Notebook/Lab_581

2012-11-07T16:17:32Z

Autocreate 2012/11/07 Entry for User:Samiye_Yaman/Notebook/Lab_581

New page

{|{{table}} width="800"
|-
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>      </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|-
| colspan="2"|


==Description==

*The course is designed by American University to experiment different aspects of PVOH films.

*During the course PVOH films with different molecular weight will be produced. Effects of cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.

*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.

←Older revision		Revision as of 16:35, 7 November 2012
Line 37:		Line 37:
	==Data==		==Data==

-	'''~~Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''~~	+	'''DSE Results'''
-		+
-	*Before cross-linking	+
-		+
-	*The film shrunk and look more brittle.	+
-		+
-	*More intense green color.	+
-		+
-	~~[[Image:2012-10-31_11.23.11.jpg\|500px]]~~	+
-		+
-		+
-	~~'''FTIR~~ Results'''	+
-		+
-	~~[[Image:1g22000PVOHcrosslinked.png\|500px]]~~	+
-		+
-		+
-	~~[[Image:1g22000PVOHH3PO4MaleicAcid.png\|500px]]~~	+
-		+
-	~~[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH22000H3PO4.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000HCl.png\|500px]]~~	+
-		+
-	~~[[Image:1gPVOH100000HClcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:Halfg22000PVOHgluteraldehyde.png\|500px]]~~	+
-		+
-	~~[[Image:Halfg100000PVOHcrosslinked.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH2200.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH22000H3PO4.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH100000HCl.png\|500px]]~~	+
-		+
-	~~[[Image:HalfgPVOH100000HClSuccinicAcid.png\|500px]]~~	+
-		+
-	~~[[Image:OnetenthgPVOH22000.png\|500px]]~~	+
-		+
-	~~[[Image:OnetenthgPVOH100000.png\|500px]]~~	+

	==Notes==		==Notes==