User:Abigail E. Miller/Notebook/MOF Project/2013/01/31

Metal Organic Frameworks

Main project page Previous entry      Next entry

Objective Insert content here... Bench Work made a solution of 4, 4 bipyridine 6 mg of 4, 4' bipyridine in 3 mL of DEF and 1 mL of ethanol exchange the pillar from DPNI to 4, 4' bipyridine 1:15 pm mixed 3 mL of hte above solution with 13 mg of PPF-18 4:30 pm filtered and dried the crystals see Eleni's notebook for 3 vials of reactants for synthesizing PPF-18 place the vials in the oven at 9am on 2/1/2013 to ehat for 24 hrs at 85 °C then cool to room temp over for 9 hrs. react OD2A with zinc nitrate see Matt's notebook for reactant amounts heated for 2 hrs at 130 °C let cool on bench top - some white crystals at hte bottom of hte vial heated from 1-4:30pm at 130 °C then turned off the oven and let it cool to room temp Data/Spectra Insert content here... Notes Insert content here...