User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/05
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Purification of Large-Scale Reaction Between CNP & MTT
The procedure for the reaction being discussed can be found here.
EtOAc Fraction: Image:Awl etoac fraction 100515.pdf
MeOH Fraction: Image:Awl meoh fraction 100515.pdf
The EtOAc fraction shows a clear peak at 287 (mass plus H) and 108.8 (mass plus Na). A likely next step is to run a TLC on the compound in an attempt at further purification.