User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/15

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Recombination of Old Fractions and Cleaning the Lab

Three fractions from previous points during the purification process remained. TLC was run on the three fractions, along with the two starting materials for comparison, and it was determined that each of the three fractions contained some amount of the desired product (or at least something consistent that was not either of the starting materials). The three fractions were then combined, rotovapped, and capped for later purification. Ideally, we want to purify this so that we can have a stock of the compound AL1 if the NIH researchers decide they need more of this.

My bench area was also cleaned.



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