User:Dominique Brager/Notebook/481 Notebook/2016/09/21

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Objective

30% clay beads prepared

Weighed columns

  • activated Carbon
  • 10%
  • 20%
  • 30%

Description

  • Data for the columns prepared for MG adsorption next time. Columns were filled approximately halfway with beads.


  • 30% clay beads:

1.2505g PVA

1.25g PVA/7 * 3 = 0.0.5357g

0.5357g Bentonite * 97ml solution/3g bentonite = 17 mL bentonite solution

55mL solution - 10 mL bentonite solution - 15mL HCL: 23 mL H2O

  • Create a solution of with PVA, bentonite solution and water
  • Place this solution on a hot plate and heat/stir until everything has dissolved.
  • Add 5 mL of this solution to a 50 mL solution of ethyl acetate dropwise stirring at 380 rpm.
  • Add 0.5 mL of glutaraldehyde and stir at 400 rpm.
  • After 7 minutes, add 7 mL of sodium bicarbonate and stir for 30 seconds.

Data

Column Volumes (g)
Activated Carbon 10%
Empty Dry with Clamp 20.1234 20.1105
Clamp 4.13733 4.1437
Empty Dry 15.98607 15.9668
Empty Wet 16.38975 16.3416
Beads in Column with Clamp 22.3344 21.95
Column with Beads 18.19707 17.8063
Beads 1.8075 1.4647

Notes

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