User:Elaine Marie Robbins/Notebook/MOF/2012/07/09

From OpenWetWare
Jump to navigationJump to search
Synthesizing TBAPy Main project page
Previous entry      Next entry

Methods

  1. Rotovap.
  2. Recrystallize with hot toluene.
  3. Filter out crystals with nylon filter paper.
    • Yield = 2.9799 g
  4. Dissolve 1 g of solid in 100 mL THF/dioxane/H2O.
  5. Add 20 mL of 2 M NaOH.
  6. Stir under reflux at 85°C overnight.


Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Elaine_Marie_Robbins/Notebook/MOF/2012/07/09&oldid=1010515"