User:Elaine Marie Robbins/Notebook/MOF/2012/07/09

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Synthesizing TBAPy Main project page
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Methods

  1. Rotovap.
  2. Recrystallize with hot toluene.
  3. Filter out crystals with nylon filter paper.
    • Yield = 2.9799 g
  4. Dissolve 1 g of solid in 100 mL THF/dioxane/H2O.
  5. Add 20 mL of 2 M NaOH.
  6. Stir under reflux at 85°C overnight.


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