User:Elaine Marie Robbins/Notebook/MOF/2012/07/19

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PPF-20 with DNA Bases Main project page
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Methods

  1. Mix 1 mg PPF-20 and 1 mg adenine/guanine in 0.75 mL DEF and 0.25 mL EtOH in a cuvette.
  2. Take UV/Vis data over 3 hr.
  3. Synthesize In2(OH)2TBAPy.
    1. Mix 12 mg In(NO3)3•9H2O and 10 mg TBAPy in 4 mL DMF/dioxane/H2O (2/1/1).
    2. Add 10 μL concentrated HCl.
    3. Heat at 85°C for 12 hr.

Data

  • Powder XRD data compiled for TBAPy and In2(OH)2TBAPy:
Image:12-07-19 PXRD of TBAPy and InTBAPy.png
Image:12-07-19 PXRD of InTBAPy magnified.png
  • Powder XRD data compiled for PPF-20 with adenine:
Image:12-07-19 PXRD of PPF20 w adenine.png
Image:12-07-19 PXRD of PPF20 w adenine magnified.png
  • Powder XRD data compiled for PPF-20 with guanine:
Image:12-07-19 PXRD of PPF20 w guanine.png
Image:12-07-19 PXRD of PPF20 w guanine magnified.png


  • UV/Vis of PPF20 and adenine over time:
Image:12-07-19 uvvis of PPF20 + adenine over time.png
Image:12-07-19 uvvis of PPF20 + adenine over time magnified 1.png
Image:12-07-19 uvvis of PPF20 + adenine over time magnified 2.png
  • UV/Vis of PPF20 and guanine over time:
Image:12-07-19 uvvis of PPF20 + guanine over time.png
Image:12-07-19 uvvis of PPF20 + guanine over time magnified 1.png
Image:12-07-19 uvvis of PPF20 + guanine over time magnified 2.png


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