User:Matthew R Skorski/Notebook/471 - Exp BioChem/2015/09/23

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Objective To analyse the AUNP Lysozyme fibers using DSC, Powder XRD, and FTIR. Description Instructions for the day can be found here. Prepping AUNP fibers Poured 10 of the 5mL samples of ANUP fibers into 5 15 mL falcon tubes, 2 5 mL samples to a tube. Centrifuged the tubes for 5 minutes at 4000 rpm in the centrifuge Prepping DSC Samples Sample 1: AUNP Fiber Pan & Lid: 51.37 mg Sample: 3.49 mg Together: 53.73 mg Sample 2: AUNP Fiber Pan & Lid: 50.80 mg Sample: 4.43 mg Together: 53.74 mg Sample 3: Lysozyme Pan & Lid: 51.27 mg Sample: 3.04 mg Together: 54.38 mg Sample 4: Lysozyme Pan & Lid: 50.71 mg Sample: 3.63 mg Together: 54.44 mg Running DSC Samples Steps for DSC Samples equilibrate at 20°C ramp 5°C/min to 100°C hold for 3 min ramp 5°C to 200°C isotherm for 1 min repeat to #2 2 times Running DSC Scans GET CONDITIONS Running FTIR GET CONDITIONS Results ASK HARTING HOW TO MAKE UP THIS DATA