User:Eleni N. Kalivas/Notebook/CHEM-571/2014/02/05: Difference between revisions

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# Data Analysis of UV-vis and fluorescence spectroscopy  
# Data Analysis of UV-vis and fluorescence spectroscopy  


=Protocol for New synthesis method=
==Protocol for New synthesis method==
This protocol was taken from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/02/03|Matt Harting's]] notebook
This protocol was taken from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/02/03|Matt Harting's]] notebook


Revision as of 13:56, 4 February 2014

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Protocol

  1. Synthesize new nano crystals
    1. Are any new ligands available for synthesis?
  2. Attempt new synthesis method
  3. Data Analysis of UV-vis and fluorescence spectroscopy

Protocol for New synthesis method

This protocol was taken from Matt Harting's notebook

  1. To a 3-necked flask is added
    1. 25mL of 20mM L-cysteine
    2. 25mL of 20mM BSA
    3. 5mL of 100mM ZnSO4 (0.5 mmol)
    4. 5.437mL of 10.3mM MnCl2 (0.056 mmol)
    5. The pH of this mixture is adjusted to 11 with ~1M NaOH (should be on the order of 60uL)
  2. This mixture is stirred under Ar (I'll use N2) for 30 minutes
  3. 5.505mL of 101mM Na<usb>2S is quickly added.
  4. The solution is stirred for 20 minutes
  5. The solution is then aged at 50C under air for 2 hours.



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