User:Keyun Wang/Notebook/Experimental Biological Chemistry I/2013/01/29: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Experimental Biochemistry II</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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== | ==Purpose== | ||
* | * Start making sample Silver film with proposed protocol | ||
==Procedure== | |||
* 2.87g of AgNO<sub>3</sub> was weighted out and placed in a 50mL Erylenmeyer flask. | |||
* 0.3g of Laponite clay was weighted out and placed in same Erlenmeyer flask as above. | |||
* The 2.87g of AgNO<sub>3</sub> was calculated in the following ways: | |||
Cationic exchange capacity of Laponite: 0.55 milliequivilient/gram | |||
Weight % of silver to be exchanged in Clay: 95% | |||
Calculation is shown as follows: | |||
0.3 g LMT × (55 meqv/100 g LMT) × (1 mol Ag<sup>+</sup>/1000 meqv) × (107.86 g Ag<sup>+</sup>/1 mol Ag<sup>+</sup>) × (1 mol Ag<sup>+</sup>/1 mol AgNO<sub>3</sub>) × (1 mol AgNO<sub>3</sub>/169.87 g AgNO<sub>3</sub>) × 95% = 0.00009953 g AgNO<sub>3</sub> | |||
* 10mL of 50/50 water/ethanol solution was made by combining 5mL of water and 5mL of ethanol in a 10mL graduated cylinder. | |||
* 10mL of water/ethanol solution was poured into Erylenmeyer flask along with a stir bar. | |||
* The Erylenmeyer flask containing the solution is covered with aluminum foil and placed on stir plate under fume hood for 24 hours. | |||
==Observations== | |||
* The clay and AgNO<sub>3</sub> solution appeared white in color during stirring. | |||
Latest revision as of 22:23, 26 September 2017
Experimental Biochemistry II | Main project page Previous entry Next entry |
Purpose
Procedure
Cationic exchange capacity of Laponite: 0.55 milliequivilient/gram Weight % of silver to be exchanged in Clay: 95% Calculation is shown as follows: 0.3 g LMT × (55 meqv/100 g LMT) × (1 mol Ag+/1000 meqv) × (107.86 g Ag+/1 mol Ag+) × (1 mol Ag+/1 mol AgNO3) × (1 mol AgNO3/169.87 g AgNO3) × 95% = 0.00009953 g AgNO3
Observations
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