User:Marjan Dolatmoradi/Notebook/Chem671/2017/10/17

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Preparation of reducing agent stock solution

  • 10 mL of 100mM reducing agent stock solution:

0.01 L* 100*-3 mol/L* 180.16 g/mol = 0.18016 g Fructose

0.01 L* 100*-3 mol/L* 180.156 g/mol = 0.180156 g Galactose

0.01 L* 100*-3 mol/L* 168 g/mol = 0.168 g Chitosan + 0.168 g* 4.75 mL/g = 0.798 mL HCl

0.01 L* 100*-3 mol/L* 342.296 g/mol = 0.342 g Sucrose

0.01 L* 100*-3 mol/L* 176.1 g/mol = 0.1761 g H2Asc

-4 mL of cellulose solution --> 2.5 mM

AuNP solution preparation

-0.1 mL HAuCl4 + 0.1 mL 100 mM reducing agent + 3.8 mL H2O.

-About Cellulose, 0.1 mL HAuCl4 was added to 3.9 mL of that.

-7 test tubes were placed in water bath at 80 0C till color changes were observed.


Result