User:Abigail E. Miller/Notebook/MOF Project/2013/01/23

Metal Organic Frameworks

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Objective exchange DPNI for adenine in PPF-18 (PPF-18A) powder XRD of PPF-18A filter, collect and powder XRD of attempt to synthesis MOF with DO2A Bench Work 9am removed DO2A plus zinc reaction from the solution yellowish solution with white suspension white solid material on bottom and sides of vial let cool to room temp on the bench t also removed PPF18 and PPF18A samples from powder XRD sensor, went off due to over heating of the X ray source exchanging DPNI for adenine mixed 0.5 mL of ethanol and 1.5 mL DEF added 0.0070 mg adenine, but it did not all dissolve collected UVVis spectrum of solution Weight of PPF18 paper 0.1332 g paper plus PPF18 0.1528 g after putting in 10mL beaker, paper 0.1332 g Some loss of material to static 10:20am added 1mL of adenine solution to PPF18 waiting 3 hrs filtered material from DO2A and zinc reaction 1:30 pm filtered PPF18 with adenine filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18 washed with DEF Data/Spectra Insert content here... Notes Insert content here...